GCMS analysis results for sample AE09572, May 2002

NYC 9/11 Public Portal Document

‘Data File C:\MSDCHEM\1\DATA\050902\9571.D Vial: 8 Acq On 9 May 2002 8:59 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 5-Hexen-2-one Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

7.73 0.28 ug/L 334507 1,4-Dichlorobenzene-d4 9.94

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 5-Hexen-2-one 98 C6H10O 000109-49-9 12, 2 1,4-Butanediamine 88 C4H12N2 000110-60-1 Y0 3 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 10 4 Acetone__________ 58 C3H60 000067-64-1 9 Abundance Scan 792 (7.733 min): 9571 .D (-787) (-) m/z 43.10 100.00% 43

5000 58 87 ■ ■ i ■ ■ ■ ■ i 1 1 ‘ ' i ■ ■ 1 ‘ i 98

Tl/Z-> Of - 10 20 30 36 . 1 40 50 60 -— 70 80 90 100 +Al— 7.40 m/ z 7.60 58.10 7.80 8.00 33.23% Abundance #5001:5-Hexen-2-one 43 MWWWWMMww 5000 7.40 7.60 7.80 8.00 55 m/z 87.10 22.60% 15 27 Of 111,20, .11,32 38,1 —I 60 65 71 77 83 50 । । ■ ■ ■ ■ l■■ • > ■ ■l ■ ' 98 ■ > i ■ • • i । ■ Tl/Z-> 10 20 30 40 50 60 70 80 90 100 Abundance #739:1,4-Butanediamine 33 ............... t ............ 7.40 7.60 7.80 8.00 5000 m/z 59.10 15.86% 43

18 12 . J 01 TTITT 2511 18 1—— 54 59 70 79 88 Tl/Z-> 10 20 30 40 50 60 70 80 90 100 Abundance #110033:4-Penten-2-one, 4-methyl- 43 7.40 7.60 7.80 8.00 m/z 83.10 14.75%

5000

28 83 55 98

m/z-> 0 1 ■ i 10 ■ 1 ■ ■ i 1 20। ., ill, ।, 30 40 . ' I 1,1) I ' " -- !50 60 70 80 90 100 7.40 7.60 7.80 8.00

9571.D 050102.M Mon May 13 11:48:17 2002 Page 5

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