GCMS analysis results for sample AE09576, May 2002

NYC 9/11 Public Portal Document

. Data File : C:\MSDCHEM\l\DATA\050902\9576.D Vial: 12 Acq On : 10 May 2002 12:15 am Operator: Mclean Sample : 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 Hexanal Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.11 0.22 ug/L 270702 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanal 100 C6H120 000066-25-1 38 2 Hexanal 100 C6H120 000066-25-1 32 3 Hexanal 100 C6H120 000066-25-1 25 4 2-Buten-l-amine, N-butyl-, (Z) - 127 C8H17N 062337-87-5/16 Abundance Scan 346 (5.112 min): 9576. D (-341) (-) m/z 56.20 100/00% 44 55 129

5000 71 82

I, i ■ ■ ■ ■ । । । 35 4.80 5.00 5.20 5.40 0! ■1111'11'■■■ i1 ■1 'T1 --- * 111 > । ‘ । ■ i ■ ■ - > । ■ 1111 1 *11 m/z 44.10 91.56% n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #110561: Hexanal 44

Wu, 56 wAMW 5000 27 1 1 ' I ' ' ' ' I ' ' ' ' I ' ' 1 ' I ' * ' ' I 4.80 5.00 5.20 5.40 72 m/z 41.10 83.75% 82 , 38 50 I 62 | । — 98 Of ■ ■ i r ■ ■ ■ i ■ ■ 1 I'1 ' I" +++ l| 1 1 1’11’181 ' i ■ ■ ■ ' I ■ ' ' ■ i ■ ' ' ' i ■ • ' ' i ■ ' 1 ' 1 ■n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance 44 56 #10785: Hexanal woolom 4.80 5.00 5.20 5.40 5000 m/z 128.90 75.95% 29 72 82

m/z-> 0 -+34 +50.11654 10 20 30 40 50 60 70 | ■ 1 ' I’l’t । 80 94100 i। 90 100 । । । 110 120 । 130 । — Abundance #110562: Hexanal 44 4.80 5.00 5.20 5.40 56 m/z 57.10 64.20%

5000 27 72 82

miz-> 15 0 '1111411111' 10 20 30 +434 50 40 ' "r1'1 1.65 1 50 1 60 70 80 100 ■ i . . ■ ■ i - ■ . ■ i > ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ . i 90 100 110 120 130 4.80 1 1 1 i1 ' p 1 ■ i 4 ■ i 5.00 5.20 5.40

9576.D 050102.M Mon May 13 11:51:37 2002 Page 5

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