GCMS analysis results for sample AE09334, May 2002

NYC 9/11 Public Portal Document ILULCLY OCCLwi wpOulit L\CDU

Data File C:\MSDCHEM\1\DATA\050202\9334.D vial : 12 Acq On 2 May 2002 8:38 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 Hexanal Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

5.11 0.32 ug/L 226855 1,4-Dichlorobenzene-d4 9.94

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanal 100 C6H120 000066-25-1 52 2 Hexanal 100 C6H120 000066-25-1 5, 3 Hexanal 100 C6H120 000066-25-1/50 4 Hexanal 100 C6H120 000066-25-1 50 Abundance Scan 346 (5.112 min): 9334.D (-339) (-) m/z 44.15 100.00% 4|4 56

5000 129 A/WMMWW Mpsu 72 82 ‘‘I’ ‘t ′ 11 । >] । । i । । I r .--j

50 4.80 5.00 5.20 5.40 - > i ■ ■ ■ ■ । - ■ • ■ । ■ ■ ■ ■ । ' _L I ■ 1 ' 1 1 ‘ ' । 1 | I I I I | I I । । | r 1 >> । < 1 1 > । । 1 । । ' m/z 56.10 96.29% m/z-> Abundance 10 20 30 40 50 60 70 #10785: Hexanal 80 90 100 110 120 130 I 44 56

5000 ' ' ' 1 1 1 1 ' 1 1 ' 1 1 1 1 ' ' ' I 1 1 ' ' I 29 4.80 5.00 5.20 5.40 72 m/z 41.10 90.17% 82

m/z-> ...... . III, . 34 10 20 30 40 501 165,-1—— —L 94 100 50 60 70 80 90 100 110 120 130 1 i ■ ' 1 ' I 1 1 1 1 I r ' 1 1 i 1 ’ ■ ' i ■ 1

Abundance #110562: Hexanal 44 56 MAMAAApAAAARCTA,NAAAAOAAAL—AAADY 4.80 5.00 5.20 5.40 5000 m/z 43.10 60.51%

NM 27 72 82 15 TTTPTT I 50 +—M P+ 38 | 45514 | 100 r ■ ■ i 1 ■ 1 ■ i ■ ' 1 1 i ' 1 ' 1 i ■ 1 ' 1 i ' ■ ■ ■ i 1 NAMyM/ws”k /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #110563: Hexanal 1 ' 1 1 ' 1 1 ' I ’ 1 1 1 1 1 1 1 1 I ' 1 1 1 I 44 4.80 5.00 5.20 5.40 56 m/z 57.10 53.10% 27 y 5000 A 72 82 ■ ■ i 1 1 • ■ i 1 ' 1 137 ' i ' 1 1 ' 1 1 50 T774+ — — 177.7 ’ I ' ’ ' ' I 1 ' ' 1 I ' ' 1 ' I ' ' 1 ■ । 1 1 1 1 । 1 1 ■ 1 । ■ 1 1 ■ । 1 1 1 ■ i /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 4.80 5.00 5.20 5.40

9334.D 050102.M Mon May 06 13:58:38 2002 Page 5

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