Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09572 conducted on May 14, 2002.
NYC-WTC_000023063–000023075Folder label: “GCMS X 5/8/02 A 5/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
• Data File C:\MSDCHEM\1\DATA\050902\9571.D Vial: 8 Acq On 9 May 2002 8:59 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L
Peak Number 3 Phenanthrene, 9-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.
22.58 0.35 ug/L 606545 Phenanthranene-dl0 22.96
Hit# of 5 Tentative ID MW MolForm CAS# Qual 000883-20-5 53-9 l Phenanthrene, 9-methyl- 192 C15H12 2 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 53/“ 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 4 Phenanthrene, 3-methyl- 192 C15H12 000832-71-340 Abundance Scan 3319 (22.580 min): 9571. D (-3307) (-) m/z 192.10 100.00% 192
5000- / A 40 54 70 82 I 106 120 I 160 22.20 22.40 22.60 22.80 23.00 0 . .............. 11.111 r r ■ ■ । ■ u ■ | ■ 11111 nj. JI-. । > .7. ।... 11 ■ ■ < .. .......... — m/z 191.10 19.08% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192
5000 22.20 22.40 22.60 22.80 23.00 m/z 146.10 15.04% 96 165 i i 29 39 51 63 74 83 | 115 126 139 152 1 176 0V mpmmmmmmpmmmmmHt 111’3 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192 ----- 22.20 22.40 22.60 22.80 23.00 5000 m/z 193.10 13.13%
69 109 134
/z-> 0 45 1111111111111 It' ।11111J -MH । 82 90 1 122> | 148 160 -P11111-" । "' 11| "'i'p' 111'"FTT TTjn 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 22.20 22.40 22.60 22.80 23.00 161 m/z 96.10 11.27%
5000 77 91 121 149 177 103
n/z—> O-PP .ZJ.I, 11‘ I Ll .I,.„1m11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 138 4 22.20 22.40 22.60 22.80 23.00
9571.D 050102.M Mon May 13 11:48:17 2002 Page 6
NYC-WTC_000023073
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000023517
Laboratory report page showing GC/MS analysis for sample AE10817 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023156
Laboratory report showing GCMS analysis of sample AE09576 conducted on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023107
Laboratory report showing GCMS analysis of sample AE09574 conducted on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024100
Laboratory report detailing GCMS analysis of sample AE10897 conducted on May 21, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023472
Laboratory report showing GC/MS analysis results for sample AE10163 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023179
Laboratory report showing GCMS analysis of sample AE09577 conducted on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023454
Laboratory report showing GC/MS analysis results for sample AE10160 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023871
Laboratory report showing GC/MS analysis of sample AE10901 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024167
Lab notes regarding low recovery in sample AE10206 requiring re-extraction and successful re-analysis on May 21, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025332
Fragmented document containing GC/MS data from May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046081
Gas chromatography-mass spectrometry report for sample AE10814 showing detection of unknown compounds and surrogate recovery.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044708
Laboratory report documenting GCMS analysis of sample AE09336 conducted on May 8, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000022961
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000022962
Fragmentary record containing a document identifier and date from the DEP GCMS analysis series.
Filed in the same folder
NYC-WTC_000022965
Laboratory report of a GCMS blank run conducted on May 14, 2002, showing non-detect results for various compounds.
Filed in the same folder
NYC-WTC_000022990
Laboratory report documenting GCMS calibration verification analysis conducted on May 14, 2002.
Filed in the same folder
NYC-WTC_000022994
Laboratory report of GCMS reference standard analysis conducted on May 14, 2002, showing recovery percentages.
Filed in the same folder