GCMS analysis results for sample AE09335, May 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\9335.D Vial: 13 Acq On 2 May 2002 9:27 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 18 9-Octadecene, 1,1-dimethoxy... 'Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T.

39.00 0.21 ug/L 249491 Perylene-dl2 34.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 9-0ctadecene, 1,1-dimethoxy-, (Z)- 312 C20H40O2 015677-71-1 4/ 2 1-Nonanol, 2,2,3,3,4,4,5,5,6,6,7... 450 C9H3F17O 000423-56-3 1 3 Furo[3,4-b]furan-2,6(3H,4H)-dion... 266 C15H2204 020223-76-11 4 2-(l-Cyano-3-methyl-but-2-enylam... 188 C10H12N4 1000187-67-1 1 Abundance Scan 6113 (38.997 min): 9335.D (-6102) (-) m/z 40.10 100.00% A*ARRRAA 43

5000 95 122 161

hl i 1,, I , ............................... 67 231 191 )—T 38.60 38.80 39.00 39.20 39.40 U ' 1 I1 1 i | r—I । । [ i । । । । i । । । ' "| । > । । । । । । i । । । । । [ r m/z 95.10 42.11% m/z->0 50 100 150 200 250 300 350 400 450 Abundance #108358: 9-Octadecene, 1,1-dimethoxy-, (Z)- "/ 31 71

5000 38.60 38.80 39.00 39.20 39.40 m/ Z 122.2 0 38.60% . I l 11.25,152/184 222 248 280 ............................ m/z-> 0 50 100 150 200 250 300 350 400 450 Abundance #1088:1-Nonanol, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptad... 31 u i 1 ' 1 ' i ' ' 38.60 38.80 39.00 39.20 39.40 5000 m/z 161.20 38.38%

69 131 1/1.101 | 151 181202 231 263 295 323345 381 414436 । । । i rf —1 r i 1 r I i i [ i i f i । r I i i | i—i—i—i—|—i—i—i ! [ i i—i—i—(—r 1 m/z->0 Abundance 31 50 100 150 200 250 300 350 #1126: Furo[3,4-b]furan-2,6(3H,4H)-dione, dihydro-3-methyl... 400 450 1 38.60 38.80 39.00 39.20 39.40 m/z 107.10 35.86% 96 5000

/z-> 0 i 1 a 1,-164.191 . ............. 50 [ r ‘ 68 i i

100 । i 124 i । ।

150 । i i i i

200 । t t i ।

250 । । । । i

300 । । f i ।

350 । i r I J

400 | I i i i

450 । i ii„. ii in 38.60 38.80 39.00 39.20 39.40

9335.D 050102.M Mon May 06 14:00:04 2002 Page 23

NYC-WTC_000044698