NYC-WTC_000024014
Laboratory report showing GC/MS analysis of sample AE10985 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Document / 32 pages
GCMS analysis results for sample AE09571, May 2002
Machine-extracted title · confidence 100%Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09571 conducted on May 14, 2002.
NYC-WTC_000023023–000023054Folder label: “GCMS X 5/8/02 A 5/9/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050902\9570.D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 18 4,8,12,16-Octadecatetraen-l... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 32.94 2.22 ug/L 3127520 Perylene-dl2 34.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4,8,12,16-Octadecatetraen-l-ol, ... 318 C22H380 1000142-00-0 43 2 8-Thiabicyclo[4.3.0]nonane S-oxide 158 C8H140S 1000215-10-0/38 3 Bicyclo[2.2.1]heptane-2,3-dione,... 166 C10H14O2 000465-29-222 4 Cyclobutene, 1,2,3,4-tetramethyl- 110 C8H14 090346-45-5 22 Abundance Scan 5082 (32.939 min): 9570.D (-5076) (-) m/z 69.15 100.00% 63 95 MMMMMyMoMn 121 5000 141 168 192 217 260 281 •43 372
miz-> 0- ...... 1 ' I " " P'1 T‘ +AlLhl —L —L ’1’44' । ■ II " i " ■' i1 " ■ i " '' r ' ■11" ’T :20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 32.60 32.80 33.00 33.20 m/z 95.10 100.00% Abundance #41281: 4,8,12,16-Octadecatetraen-1-ol, 4,9,13,17-tetramethyl 41 95 69
5000 32.60 32.80 33.00 33.20 121 m/z 67.10 91.33% , 149
miz-> 0 4M4444++ 20 40 177 205 231249 275 308 TT 1111' r ‘ I I'' I'''' I'11' I'''' I'''' 11''' I 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 "NMWMMWMMAvNANYpMMAay/ Abundance #41201:8-Thiabicyclo[4.3.0]nonane S-oxide 67 95
32.60 32.80 33.00 33.20 5000 m/z 109.10 71.43% 141158 NMWNPMMMMyMAAp/Awn OU J l " •' I ‘ ‘ I ‘ TT—TTTTTTTTTTTTTTTTTTTTTTTTTTWWTITTTT m/z—> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance! #118186: Bicyclo[2.2.1 ]heptane-2,3-dione, 1,7,7-trimethyl- 95 32.60 32.80 33.00 33.20 41 69 m/z 55.10 63.27% 5000 M’W"WWMWWM 138 166
/z—> oM — 44 a 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 32,60 32.80 33.00 33.20
9570.D 050102.M Mon May 13 11:46:50 2002 Page 24
NYC-WTC_000023051
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NYC-WTC_000045662
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
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1 shared topics · similarity 0.993
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Laboratory report detailing GC/MS analysis of sample AE10609 including surrogate recovery data in May 2002.
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