GCMS analysis results for sample AE09571, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050902\9570 .D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 17 3-Hydroxypyridine-2-carboxa... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

32.82 2.18 ug/L 3060900 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hydroxypyridine-2-carboxamide, ... 152 C7H8N202 1000191-74-0 3 2 1,3-Butanedione, 1-(2-furanyl)- 152 C8H803 025790-35-6 22 3 2-Oxatricyclo[3.3.1.13,7]decane,... 152 C1OH160 006508-22-112 4 2(1H)-Naphthalenone, octahydro-1... 180 C12H20O 022738-31-4 10 Abundance Scan 5062 (32.821 min): 9570.D (-5059) (-) m/z 95.10 100.00%

69 95 nAPMAMMvwpAMurvty 5000 152 109 125 203 217 233 281 39 189 165 32.40 32.60 32.80 33.00 33.20 0- ■ i' ■ ‘ ■ i ■ ' 56 i ■ _ । 1 II Illi 1111 ' 1 11 111 1 1 1 ' 1 r I ' ’ 1 m/z 69.10 67.67% n/z-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 #41595:3-Hydroxypyridine-2-carboxamide, N-methyl vMArMWywhMbponpl 95

152 5000 123 32.40 32.60 32.80 33.00 33.20 39 67 m/z 71.10 61.04% 0 —2029154 —81.4M9 1:36 ■ i ■ ■ ' ■ i ■' ' ■ I 1 ' 1 ‘ i ■ ■ ' 11 ■ ■ '' i ■ ■ ' ‘ i ' 1 A"h-kAHwy" n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41458:1,3-Butanedione, 1-(2-furanyl)- 95 110 32.40 32.60 32.80 33.00 33.20 43 5000 69 m/ z 58.20 49.21%I 152 137 27 on 124 0- .ll. nd n • 1. 94 । । | Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #118194: 2-Oxatricyclo[3.3.1.13,7]decane, 1-methyl- ■ 1 i 1 ■ ■ z r ■ ■ 95 32.40 32.60 32.80 33.00 33.20 m/z 152.10 45.90%l

5000 152 43 79 109 42

m/z-> 0 20 l —6. IM. 1,4423137 40 60 80 100 120 140 160 180 200 220 240 260 280 i ■ 1 ■ * i ■ • 1 1 I ' ' ' ' I ' ' 32.40 32.60 32.80 33.00 33.20

9570.D 050102.M Mon May 13 11:46:49 2002 Page 23

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