GCMS blank analysis results for sample AE09329, May 7 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050202\0429LB.D Vial: 6 Acq On 2 May 2002 3:38 pm Operator: Mclean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 6 1,1-Cyclopropanedicarboxamide Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 34.97 0.31 ug/L 134890 Perylene-dl2 34.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,1-Cyclopropanedicarboxamide 128 C5H8N2O2 1000224-97-7/4 2 4H-1,2,4-Triazol-4-amine 84 C2H4N4 000584-13-44 3 2-Butenedioic acid, 2-methyl-, (Z)- 130 C5H604 000498-23/7 3 4 Butanedioic acid, methylene- 130 C5H604 000097-65-4 ■ 3 Abundance Scan 5427 (34.966 min): 0429LB.D (-5426) (-) m/z 83.90 100.00% 84 259 208 96 128

5000

34.60 34.80 35.00 35.20 35.40 40 ■111 111111 1 11111' । 1 i 1 1 ' 1 i 1 1 1 1 1 1 1 1 ' i 1 1 1 I 1 1 ' ' I 1 1 * ’ I 1 ' m/z 259.10 92.67% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #1278:1,1-Cyclopropanedicarboxamide 39

5000 84 128 34.60 34.80 35.00 35.20 35.40 53 68 111 m/ Z 2 08.00 72.84%

/z—> — 20 40 -4 "—7 1 97 ], 60 80 1 ■' ■ I ' 11 1 1 1 100 120 ■ ■ । 140 ■ i ■ > ■ > । ■ 1 ■ ■ i > ■ - ■ । । । ■ r । ■ ■ ■ ■ । 160 180 200 220 240 260 ■

Abundance #107976: 4H-1,2,4-Triazol-4-amine 23 84 114/ yronuanton 34.60 34.80 35.00 35.20 35.40 5000 m/z 96.20 65.52% I

— 69 42

Tl/Z--> 120 - 40 60 80 57,17 100 120 140 160 180 200 220 240 260 4

Abundance #1348: 2-Butenedioic acid, 2-methyl-, (Z)- ■ i 1 1 1kt 39 34.60 34.80 35.00 35.20 35.40 86 m/z 128.00 64.66%

5000 68

J 1 53 _ _ I..’, J. , 44 IT [ I I I I | I I I I T I I | I 112 130 I r I | । « > < | । I । > | > I i I | । । r Pr I I I [ I I II | I I I 11*1

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 34.60 34.80 35.00 35.20 35.40

0429LB.D 050102.M Mon May 06 10:58:32 2002 Page 9

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