GCMS blank analysis results for sample AE09329, May 7 2002

NYC 9/11 Public Portal Document Library searcn compound Report

Data File C : \MSDCHEM\ 1 \DATA\ 050202\042 9LB . D Vial: 6 Acq On 2 May 2002 3:38 pm Operator: Mclean Sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Benzene, 1-[(4-ethoxyphenyl... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

34.91 0.38 ug/L 165554 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, 1-[(4-ethoxyphenyl)ethy... 264 C19H20O 039969-29-4 5 2 p-Terphenyl, 4-chloro- 264 C18H13C1 001762-83-0 3 3 1OH-Phenoxaphosphine, 2-fluoro-l... 264 C13H10FO3P' 037041-12-6 3 4 Tricyclo[10.2.2.25,8]octadeca-5 ,... 264 C20H24 024777-38-6 3 Abundance Scan 5417 (34.907 min): 0429LB.D (-5416) (-) m/z 129.60 100.00% 129 207 264 281 49 5000

34.60 34.80 35.00 35.20 - m/z 207.00 97.36% i ' 1 1 1 i ' i 1 1 1 1 I ' 1 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #84924: Benzene, 1 -[(4-ethoxyphenyl)ethynyl]-4-propyl- 207 WMpHwirH 235 264 29 5000 178 34.60 34.80 35.00 35.20 152 m/z 2 64.10 93.58% 165

m/z-> 15 ■ 1 ■■ । '

20 43 63 76 89 115.139 — Il i 191 . 220 1 | 1 111 | ′ 1 ' 1 | > r । ' | i ' > ■ | I I i - | i

40 60 80 100 120 140 160 180 200 220 240 260 ' 280 I 1 11 ' i 1 ■ ■ । 1 1 i 1 1 ' ‘ I 1 1 i 1 '

Abundance #95157: p-Terphenyl, 4-chloro- 264 1 111/nl ’ ] 1BB I I I I I < I I I I I I

34.60 34.80 35.00 35.20 5000 m/Z 281.00 70.57% 228

..... 51.64,77 100113 132 152 176189292215 J1 ri i " i 249 'i' i i 17 j i i i । । f i i i । i t r r | i 1 1 i 1 1 "UI ri 1 1 i 1 1 ■ 1 I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #95107:10H-Phenoxaphosphine, 2-fluoro-10-hydroxy-8-methyl... 264 34.60 34.80 35.00 35.20 m/z 261.10 63.77%

5000

199 107 ■ i ■ 1 1 1 i ■ ■ 1 1 i 1 ' 1 ' i 1 ' 1 1 i ' 1 1 i 1 ' 1 1 i ' ■ ■ ■ r 1 1 1 i ‘ I. 246 ’ 1 I ' 1 1 ' i ' 1 1 1 i 1" 1 1 i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20

0429LB.D 050102.M Mon May 06 10:58:32 2002 Page 8

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