GC/MS analysis results for sample AE11412, May 28 2002

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Laboratory report showing gas chromatography/mass spectrometry results for sample AE11412 analyzed on May 28, 2002.

NYC-WTC_000025257–000025273

Folder label: “GCMS X 5/15/02 A 5/18/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051702\11410.D Vial: 19 Acq On : 18 May 2002 4:16 am Operator: Mclean Sample : 5/15 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.41 ug/L 555774 Phenanthranene-dl0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 80 3 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 42 4 4-Methyl-2-(3-fluorophenyl)pyrim. .. 188 C11H9FN2 076128-66-0 42 Abundance Scan 3409 (23.109 min): 11410.D (-3402) (-) m/z 188.10 100.00% 188

5000 .............................................. .. 43 52 e 66 80 94 158 22.80 23.00 23.20 23.40

m/z—> 0 ■।■■■■।■■■■। > 11'1 ■ ■ i U 11 132 ।. I ■ ।. 1111... ] rl, TTTT I"...... "I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 H m/z 189.10 16.48% Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/ z 80.05 13.32% 80 94 160 66 17 30 42 52 108118 132 0 ■ i ‘ " r " 11" " 111 " i111 | | r Fr n H in +t TII—mm-unttt 146.,1.17917% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d 10 188 11. 1 . ................. . 22.80 23.00 23.20 23.40 5000 m/ z 94.10 12.57%

80 94 160 30 42 52 66 ■I 108118 0 ll""l".i|li.i|ii.l|iil.|iili|l.ll|n. I | II I , | I I , I pAryrn , [■! I I . | 132 146—44170179 — m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79745:4-Methyl-2-(4-fluorophenyl)pyrimidine - 188 22.80 23.00 23.20 23.40 m/z 187.10 11.72% 121 5000 173 67 94 39 57 | 84 133 146 161 0- ' r " 11' " ' i'111111' TTTTugu —]wn———u m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11410.D 050102.M Tue May 21 15:54:26 2002 Page 7

NYC-WTC_000025257

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GC/MS analysis results for sample AE11415, May 28 2002 · Box DEP Box 18

NYC-WTC_000025304

Laboratory report documenting gas chromatography/mass spectrometry analysis of sample AE11415 conducted on May 28, 2002.

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