GCMS analysis report sample AE09679, May 23, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052102\9679.D Vial: 17 Acq On : 22 May 2002 2:22 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 15 Anthracene -d10- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.25 ug/L 232018 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 87) 2 Phenanthrene-diO 188 C14D10 001517-22-2 87%) 3 4-Methyl-2-(3-fluorophenyl)pyrim. .. 188 C11H9FN2 076128-66-0 42 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 Abundance Scan 3402 (23.068 min): 9679.D (-3395) (-) m/z 188.10 100.00% 188

5000

80 94 43 66 160 22.80 23.00 23.20 23.40

n/z-> 0 IUTU0—0um—mu—amu mm 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 "■ i■ i' ■ “ i m/ Z 94.10 18.37% Abundance #79826: Anthracene-d1 0- 188

5000 ... . . 22.80 23.00 23.20 23.40 m/z 80.20 13.96% 80 94 160 01 17 30 42 52 6° . 108118 132 146 1. 170179.1., “T miz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188

22.80 23 00 23.20 23.40 5000 m/z 189.10 12.76%|

30 42 52 66 80 94( • 108 118 132 146 160 | 170179/ 0 111 “11 ■1 “ I"1' 11 ■1 ■ 111"1111 ■ I"1111"T111 ■111i1"11'1 "'Ii'i'it '' i 'i."ltp11r| ri 11 [Til ,■..। niz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance> #79744:4-Methyl-2-(3-fluorophenyl)pyrimidine 188 22.80 23.00 23.20 23.40 m/z 184.10 12.08%|

5000 121

173 67 94 1 1 , 82 1, 108 | 134 146 161 |; ,O-TTWTTTTTTTTTTTTPTTTTTPT 39.50 m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 22.80 23.00 23.20 23.40

9679.D 052202.M Wed May 22 11:45:39 2002 Page 18

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