GCMS analysis report sample AE09679, May 23, 2002

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GCMS laboratory report for sample AE09679 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013224–000013250

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052102\9679.D Vial: 17 Acq On : 22 May 2002 2:22 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********* * * ********************************************************** Peak Number 16 Benzene, l-fluoro-3(2-cyano... Concentration Rank 16 R.T. EstConc Area Relative toISTD R.T. 35.38 0.25 ug/L 105118 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, l-fluoro-3(2-cyanoethenyl) 147 C9H6FN 082344-56-7 5 2 1-Cyclohexen, l-cyano-4-isoprope... 147 C10H13N 1000126-45-8 4 3 Pyrido(3,4-d]pyrimidin-4(3H)-one 147 C7H5N3O ■ 019178-25-/4 4 6-Ethyl-5-[1-piperidinyl]-2,4-py... 221 C11H19N5 1000212-52-9 4 Abundance Scan 5498 (35.383 min): 9679.D (-5487) (-) m/z 73.10 1/0.00% 73 147 221 5000

40 96 281 355 MlaMnunuunCninhhnu 35.00 35.20 35.40 35.60 35.80 0- i■"• i■"■ i"■ ■ i "■ ■ i"i■ ■ ■ i■ “ ■ i ■" ■ i ■ ■ ■ ■ i■" ■ i1 • ■ ■ i ■ ■ ■ ■ i“ " i' m/z 147.00 66.40% vtz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #66081: Benzene, 1-fluoro-3(2-cyanoethenyl) 147

5000 120 MA... **I’**1** 35.00 35.20 35.40 35.60 35.80 50 75 96 m/z 221.00 57.22%

m/z—> 0-314444 7 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #65824: 1-Cyclohexen, 1-cyano-4-isopropenyI- 147 68 35.00 35.20 35.40 35.60 35.80 41 m/z 207.00 50.00% 5000 96 131

iz—> O+p M4 ■ • i■■' ■ i" " i" ■ ■ i ■ ■ “i ■" ■ i• ■ ■ ■ i ■ ■ ■ ■ i ■ “ ■ i “ “ i “ ■ ■ i ■ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #66000: Pyrido[3,4-d]pyrimidin-4(3H)-one 147 35.'oO 35.20 35 40 35.'60 35.‘80 m/z 355.00 36.24%

5000 92 50 119

n/z—> O- 44441444 ' i ■'' ■ । ■"111'" ।' “ • । ‘"11 “1 ■ i “ “ । ■1 “ 11111111 “ 11 ■" 11 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 • i ' ■ ' 1 i 1 ' 1*’’’I tE 1 ' i 1 1 35.00 35.20 35.40 35.60 35.80

9679.D 052202.M Wed May 22 11:45:41 2002 Page 19

NYC-WTC_000013247

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