GCMS analysis report sample AE09679, May 23, 2002

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GCMS laboratory report for sample AE09679 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013224–000013250

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052102\9679.D Vial: 17 Acq On : 22 May 2002 2:22 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiple: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 17 4-Thiazoleethanol, 2-(p-chl... Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T. 36.45 0.22 ug/L 93055 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-Thiazoleethanol, 2-(p-chloroph. . . 281 C13H12C1NO2S 027551-11-7 7 2 2-Amino-4-(4-chloroanilino)-S-tr... 221 C9H8C1N5 000500-42-5/5 3 Perhydro-htx-2-one, 2-depentyl-,... 281 C16H27NO3 1000126-27-9 5 4 1-Cyclohexen, l-cyano-4-isoprope... 147 C10H13N 1000126-45-8 5 Abundance Scan 5679 (36.447 min): 9679.D (-5671) (-) m/z 147.10 1/0.00% 73 147

221 5000 96 281 355 49 36.20 36.40 36.60 36.80 - 0- ‘1’1 I " “ I" ■■ i ■ “ i ■ ■ ■ ■ i “ 1 ■ i ■ • * 11 ■ ■ ■ 11 ■' ■ i ■ ■ ■ • i ■ " ■ i “ ■ • i ■ “ ■ i “ “ i ■ m/z 73.05 84.11% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #87954:4-Thiazoleethanol, 2-(p-chlorophenyl)-, acetate (e... 221

5000 43 84 36.20 36.40 36.60 36.80 m/z 221.10 54.87% 58 138

/z-> 0 114155,186. *A Hmmmmmmmp 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 238 291

Abundance #87943:2-Amino-4-(4-chioroaniIino)-S-triazine 221 T T 36.20 36.40 36.60 36.80 5000 m/z 208.90 35.38% 152 43

0 70 99 125 1 + 178193 " “' i1■■■i'■■■i ■ ■ ■11 ‘ " i1 ■■■।।■ Ji miz-> Abundance 40 60

43 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #9964: Perhydro-htx-2-one, 2-depentyl-, acetate ester 281 M ' ‘ 1 ' 36.20 36.40 36.60 36.80 m/z 96.00 31.51% 124 150 222 5000 96 178, 193 238 1 J, 67 0 -444T ff TTTTT 265 " i1 “ ■ i ‘ ■ i1 ‘ “ i" ■ ■ i ■ ■" i ■ m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 36.20 36.40 36.60 36.80

9679.D 052202.M Wed May 22 11:45:44 2002 Page 20

NYC-WTC_000013248

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