GCMS analysis report sample AE09517, May 23, 2002

NYC 9/11 Public Portal Document Library Search. Compound Report Data File : C:\MSDCHEM\l\DATA\052102\9517.D Vial: 13 Acq On : 21 May 2002 11:07 pm Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params.: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title a 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 19 3,6-Dioxa-2,4,5,7-tetrasila... Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

36.45 0.25 ug/L 130787 Perylene-dl2 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 12 2 4-Thiazoleethanol, 2-(p-chloroph... 281 C13H12C1NO2S 027551-11-7 10 3 Pentasiloxane, dodecamethyl- 384 C12H3604Si5 000141-63-910 4 1,2-Benzenedicarboxylic acid, bi... 310 C14H2204Si2 002078-22-0 10 Abundance Scan 5680 (36.453 min): 9517.D (-5673) (-) m/z 147.00 1/0.00% 147 221 73

5000 51 191 282 355 429 -LLAMMA 36.20 36.40 36.60 36.80 0- r ■ 111— '1 1 1 ,» , , ,1 II, . . I, » , I . , I..... m/z 221.05 83.22% n/z-> 50 100 150 2(X) 250 300 350 400 Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 2211

73 5000 36.20 36.40 36.60 36.80 191 m/z 73.10 82.39% 117 279

niz-> 0- 45 T‘1 50 ■ 1— 100 150 —— 249 L 200 250 .300 ■ i ‘ 1 ■ 350 i ■ ■ ' ■ i ‘ ■ 400 I ■

Abundance #87954:4-Thiazoleethanol, 2-(p-chloropheny!)-, acetate (e... 221

36.20 36.40 36.60 36.80 5000 m/z 207.00 36.41% 43 84 138 281 0- ,41 4,,/11.4157,186,4 1 240,, I, rnfe-> 50_____ 100 150 200 250 300 350 400 Abundance #115143: Pentasiloxane, dodecamethyl- 73 147 281 36.20 36.40 36.60 36.80 m/z 222.00 30.50%

5000 369 207

niz-> 0- 45 4 1 93 117, . 50 100 117.2. I, 1•1• r■ 150 200 250 300 350 L 400 36.20 36.40 36.60 36.80

9517.D 052202.M Wed May 22 11:29:29 2002 Page 22

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