GCMS analysis report sample AE09517, May 23, 2002

NYC 9/11 Public Portal Document Library Search. Compound Report Data File : C:\MSDCHEM\l\DATA\052102\9517.D Vial: 13 Acq On : 21 May 2002 11:07 pm Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 18 1-Monolinoleoylglycerol tri... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 35.38 0.32 ug/L 166981 Perylene-dl2 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual l 1-Monolinoleoylglycerol trimethy... 498 C27H54O4Si2 054284-45-6 25 2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 10 3 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 1000071-72-1 10 4 3,4-Bis-(methylthio)-quinoline 221 C11H11NS2 1000147-85/8 9 Abundance Scan 5497 (35.377 min): 9517.D (-5490) (-) m/z 73.10 100.00% 73 221 147

355 5000 281 96 429

miz-> 0- .I 50 49

100 150 1 200 250 I . 350,1..400 300 117," 1 1 I 450 35 00 35.20 35.40 35.60 35.80 m/z 221.10 86.62% Abundance #27370:1-Monolinoleoylglycerol trimethylsilyl ether 73

5000 147 207 MDAA ...................... A * I ‘ ‘ ' I ‘ ‘ 35 00 35.20 35.40 35.60 35.80 * I ‘

34 103 m/z 147.10 82.71% 281 0- LUl 44ui2E .77, +249.,+.205327,355 395 l u 429 ■ । Y . . । । 483 , i~> ] miz-> 50 100 150 200 250 300 ■ 350 400 450 Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime...

5000 73 147 281

369 TsMNvn AMMMA4..)..M.., 35 00 35.20 35.40 35.60 35.80

niz-> 0 —4+ 45

50 95 117 1 177 227 249 A 310 341 l —* . . 1 . r 1 *1" ■ ■, f ."b 1 • i ■ ' ■ ■ 1 ■ ’ ■ ■ i 1 1 1 1 I 1 1 1 1 I 100 150 200 250 300 350 400 450 Abundance #25709: N-Methyladrenaline, tri-TMS 73 35.00 35.20 35.40 35.60 35.80 m/z 355.10 51.43% 5000 355

45 207 96 267 323 0 r L 179,Iih. 147 0)4 dr 1 —4 4 - 4—r t-t—j—r-r-r-r-]—>—1—r—r—| m/z-> 50 100 150 200 250 300 350 400 450 35.00 35.20 35.40 35.60 35.80

9517.D 052202.M Wed May 22 11:29:29 2002 Page 21

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