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GCMS analysis report sample AE09517, May 23, 2002

Machine-extracted title · confidence 95%

GCMS laboratory report for sample AE09517 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013089–000013116

Folder label: “GCMS X 5/21/02 A 5/21/02

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NYC 9/11 Public Portal Document

Library Search Compound. Report Data File : C:\MSDCHEM\l\DATA\052102\9517.D Vial: 13 Acq On : 21 May 2002 11:07 pm Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 17 Heptasiloxane, 1,1,3,3,5,5,... Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T.

34.33 0.23 ug/L 117696 Perylene-d12 34.66

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H44O6Si7 019095-23-9 32 2 Silane, [[3,3-dimethyl-4-methyle... 282 C15H30OSi2 095798-07-5/10 3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 9 4 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 1000071-72-1 9 Abundance Scan 5318 (34.326 min): 9517.D (-5309) (-) m/z 73.10 100.00% 73

147 221 5000 281 355 ALAALAAAAAAAC 34.00 34.20 34.40 34.60 0- 49 ' 1 'i 1 ■ 1. .. m/z 147.10 60.56% miz-> 50 100 150 200 250 300 350 400 450 Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tet... 73

5000 207 34.00 34.20 34.40 34.60 m/z 221.10 59.86% 133 281 355

niz-> 0- —+ . 103 IL , 177 [ 1 2531 [ 50 11 1 ' f 11 1 . i । "i 100 150 200 250 । 300 - 350 । 327. 1 377399 429 । 400 i । । । i > i । 450 489 Abundance #26862: Silane, [[3,3-dimethyl-4-methylene-2-(trimethylsil... 73 34.00 34.20 34.40 34.60 5000 m/z 281.10 36.34% 147 45 105 177 209 267 J i 0- ’ r r’ * +1,4*,4 , 4 44 .? ‘ ■ i ■ ■ ■ ■ i ■ ' ■ ■ । niz-> 50 100 150 200 250 300 350 400 450 Abundance #115273: Cyclopentasiloxane, decamethyl- 73 34.00 34.20 34.40 34.60 m/z 207.00 33.24% 5000 267 355 Aoukooo/ 45 0 , I I I 96 ■ 'i ■‘ ■ 1 i' ■ 43 .4 133 165.193 :223 293 323 A ■ ' i ■ ‘ ■ i ■ 1 ■ • i nfe-> 50 100 150 200 250 300 350 400 450 34.00 34.20 34.40 34.60

9517.D 052202.M Wed May 22 11:29:29 2002 Page 20

NYC-WTC_000013113

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NYC-WTC_000013113Source: NYC Law Department, mirrored locally

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