GCMS analysis report sample AE09679, May 23, 2002

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GCMS laboratory report for sample AE09679 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013224–000013250

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052102\9679.D Vial: 17 Acq On : 22 May 2002 2:22 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ************************************ * * ******************************* Peak Number 18 2-(Acetoxymethyl) -3-(methox... Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 37.72 0.23 ug/L 96018 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-(Acetoxymethyl)-3-(methoxycarb... 282 C17H14O4 093103-70-9 16 2 7-Chloro-4-methoxy-3-methylquino... 207 C11H10C1NO> 1000213-52-2/12 3 lH-Pyrrole-2,5-dione, 1-(4-chlor... 207 C10H6C1NO2 001631-29-4/9 4 Pyridine, 1,2,3,6-tetrahydro-1-m... 207 C12H14C1N 005048-08-8 9 Abundance Scan 5895 (37.716 min): 9679.D (-5883) (-) m/z 207.00 100.00% 147 207 73

5000 282 355

40 37.40 37.60 37.80 38.00 O- ■ ■ ■I____ ■' i • ■ ' I' ! “ I' " ' 1 ‘ ‘ ' I ' ' •' I ‘ " I ' " 1 i m/z 147.10 95.01% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #84932:2-(AcetoxymethyI)-3-(methoxycarbonyl)biphenylene 207

5000 282 37.40 37.60 37.80 38.00 ‘ 151 179 m/z 73.10 74.45% 43 |. l 223239 75 98 125 266 0- ...... |. mmmmhmm AHHAR6.4 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ■ i■"■ i"" i ■ ■■ ■ i■ niz-> 20 40 Abundance #84815:7-Chloro-4-methoxy-3-methylquinoline 207 178 37.40 37.60 37.80 38.00 75 m/z 221.00 69.26% 5000

51 102 138

oV , , | Aquilik A A4k 14419 24 U I__________ • n ■ i" ■' i ■ •" i ■'' ■ i ■1 “ i11" i ■ ■" i ‘ “ i' n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #84714:1H-Pyrrole-2,5-dione, 1-(4-chloropheny!)- 17I | | | i | | M । । । 207 37.40 37.60 37.80 38.00 m/z 132.90 51.10% 54 5000

90 137 163

niz—> 0- -A47t—ll 4,1 I J 4 17%. ■ , | . l, ■ | I I ■ i | , I . i | , ■ i ■ [ ■ n-r [ ri m , ■ „

20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ■ • : ■

37.40 37.60 37.80 38.00 |l 1II

9679.D 052202.M Wed May 22 11:45:46 2002 Page 21

NYC-WTC_000013249

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