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GCMS analysis results, sample AE12477, June 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE12477 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014433–000014459

Folder label: “GCMS X 5/28/02 A 5/29/02

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Scanned page image, NYC-WTC_000014457
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052902\12477.D Vial: 19 Acq On : 30 May 2002 12:45 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 17 Anthracene-d10- Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

23.06 0.31 ug/L 283820 Phenanthranene- dl 0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 87 2 Phenanthrene-dlO 188 C14D10 001517-22-2 78 3 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 50 4 3-Amino-4-methyl -6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 Abundance Scan 3401 (23.062 min): 12477.D (-3395) (-) m/z 188.10 100.00% 188

5000 - 80 94 160 22.80 23.00 23.20 23.40

TT/z-> 40 51 0 ------ 66 TTrymryrrTTp-rrTp-rr-r^^ 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 —4ll 11111 111 m/z 184.10 17.66% Abundance #79826: Anthracene-d10- 188

5000 _mm 22.80 23.00 23.20 23.40 m/z 94.10 15.07% 80 94 160 17 30 42 52 66 , . , 108118 132 146 , |.I 170179 TDmmpmT 0 ■ ।"111 ■ it111H111.. 11! । miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ) 22.80 23.00 23.20 23.40 5000 m/ z 80.00 14.84%

80 94 160 30 42 52 66 ,1 108118 132 146 170179,1,11 0 T1WP]WWTTTTTTTTtpTmTTTmn niz-> Abundance 10 2030405060 70 8090 100110120130140150160170180190 #79745:4-Methyl-2-(4-fluorophenyl)pyrimidine 188 + 22.80 23.00 23.20 23.40 m/z 189.20 13.65% 121 5000 173 67 94 39 57 J . 84 I. 133 146 161 , 0 I1—0011——00—38———pdp——napr 1II—10—um—nnm——Ba37 li..... mfe-> 10 2030405060 70 8090 100110120130140150 160170180190 22.80 23.00 23.20 23.40

12477.D 052202.M Mon Jun 03 11:39:36 2002 Page 20

NYC-WTC_000014457

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NYC-WTC_000014457Source: NYC Law Department, mirrored locally

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