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GCMS analysis results, sample AE12477, June 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE12477 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014433–000014459

Folder label: “GCMS X 5/28/02 A 5/29/02

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Scanned page image, NYC-WTC_000014456
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052902\12477.D Vial: 19 Acq On : 30 May 2002 12:45 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********* * * ********************************************************** Peak Number 16 Phenanthrene, 9-methyl- Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 22.53 0.24 ug/L 218679 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenant hrene, 9-methyl- 192 C15H12 000883-20-5 59 2 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2 53 3 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 53 4 Benzene, l-bromo-4-chloro- 190 C6H4BrCl 000106-39-8 53 Abundance Scan 3311 (22.533 min): 12477.D (-3303) (-) m/z 192.10 100.00% 192

5000

146 160 । m 22.20 22.40 22.60 22.80

mfe-> 0 --- TTWTTPTT 54 70 82 %6 118 1 —..... + 20 30 40 50 60 70 80 90 100 110 120 130140 150 160 170 180 190 200 m/z 191.00 15.00% Abundance #81033: Phenanthrene, 9-methyl- 102

5000 22.20 22.40 22.60 22.80 m/z 146.10 14.96% 29 39 51 63 74 83 * 115 126 139 152 165 176 | 0 TETUITHmg—apmmpmgmtmBppmt ■ ■ i “ mfe-> 2030405060 70 8090 100 110 120 130140 150 160 170 180 190 200 Abundance #81023: Thiophene, 2-[2-(3-thienyl)ethenyl]- 192 0 147 22.20 22.40 22.60 22.80 5000 m/z 193.00 13.84% 45 1 ro 58 । 69| 82 _ 96 .1 105 115f . 134 — 158 27 0 T1’11-------- TTpTi 11.1» " I 1?7 miz-> 20 30 40 50 60 70 80 90 100 110120130140 150160170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyt ester 102 22.20 22.40 22.60 22.80 m/z 96.10 11.36% 5000

45 190 118 122 134 148 160 0: ----- ----- "’’I ’I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150160 170 180 190 200 22 20 22.40 22.60 22.80

12477.D 052202.M Mon Jun 03 11:39:35 2002 Page 19

NYC-WTC_000014456

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NYC-WTC_000014456Source: NYC Law Department, mirrored locally

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