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GCMS analysis results for sample AE11929, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.

NYC-WTC_000013524–000013550

Folder label: “GCMS X 5/22/02 A 5/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052302\11929.D Vial: 9 Acq On : 23 May 2002 4:29 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e ■ Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 14 Anthracene-dlO- Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

23.07 0.27 ug/L 294522 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 90 ‘ 2 Pentacyclo[7.3.1.1.(4,12).0(2,7)... 188 C14H20 1000215-61-8 50 3 4-Methyl-2-(3-fluorophenyl)pyrim... 188 C11H9FN2 076128-66-0 42 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 42 Abundance Scan 3402 (23.068 min): 11929.D (-3394) (-) m/z 188.10 100.00% 188

5000

80 94 158 22.80 23.00 23.20 23.40 40 54 132 14666 ,1 0 mpmmhpmTMTTTTTTHTT i ■ ■ ■ ■i m/z 189.10 16.92% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/ z 80.10 14.70% 80 94 160 17 30 42 52 ° .108118 132 146 )L| 170179.1,। 0 mam—mmm—phmmmm 1i n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundarice #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6>11 )tetradeca... 188

22.80 23.00 23.20 23.40 5000 79 91 m/z94.00 14.04% 55 67 105 117 131 145 159

miz-> —l -----TIPIuu 10 2030405060 70 8090 100110120130140150160170180190 173 1

Abundance #79744:4-Methyl-2-(3-fluorophenyl)pyiimidine 188 22.80 23.00 23.20 23.40 m/z 184.10 13.74%

5000 121

173 67 94

miz—> 0IWMIWTDTTTu 39 50 | , 82 |, 108 +134,146.11 Il...... ' ‘ I ’4111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160170180 190 22.80 23.00 23.20 23.40

11929.D 052202.M Wed May 29 09:49:38 2002 Page 17

NYC-WTC_000013545

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NYC-WTC_000013545Source: NYC Law Department, mirrored locally

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