GCMS analysis results, sample AE12477, June 2002

NYC 9/11 Public Portal Document Library searen compound Report:

Data File : C:\MSDCHEM\1\DATA\052902\12477.D Vial: 19 Acq On : 30 May 2002 12:45 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 18 Phthalic acid, diisooctyl e... Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 31.33 0.32 ug/L 204132 Chrysene-dl 2 30.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2 59 2 1,2-Benzenedicarboxylic acid, mo... 278 C16H22O4 004376-20-9 47 3 1,2-Benzenedicarboxylic acid, mo... 278 C16H22O4 004376-20-9 47 4 Tricyclo[3.3.1.13,7]decanone, 4-... 228 C10H13BrO 032456-48-7 9 Abundance Scan 4809 (31.335 min): 12477.D (-4797) (-) m/z 149.00 100.00% 149

5000 57 71 167 227 . ...... 43 83 113 240 31.00 31.20 31.40 31.60 I lr 0 I .... 1 . ‘*"I i !"■ i | VI I 207 I • ■ i 1 ■ ■ • i • ■ ■ ■ i 1 • ■ ■ i ‘ '• ■ ■ i • ” ■ ■ ■ ‘ T | > i ■ ‘ | rr m/z 167.00 30.31% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #66787: Phthalic acid, diisooctyl ester 149

5000 ■ ■ i • ■ ■ 1 i ■ ■ i ■ • • ■ i ■ ■ ■ ■ i 57 167 31.00 31.20 31.40 31.60 43 71 m/z 227.10 29.08% ... . 83 97.113 OfI । ... . । r . . T । . 1 ¥ I rr 1 MII I' l " l"! 132 nfz-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #67064:1,2-Benzenedicarboxylic acid, mono(2-ethylhexyl) este 149

31.00 31.20 31.40 31.60 5000 m/z 57.20 26.79% 70 167 29 41 55 83 112 0 —+A7+LL 132 II 185 199 213 228 242 256 278 , -4614saa!4t1431**11**1.a n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #123456:1,2-Benzenedicarboxylic acid, mono(2-ethylhexy!)... 149 31.00 31.20 31,40 31.60 m/z 55.10 22.24%

5000 70 41 57 167 83 112

0 1 .. 1. J I ,h II | * * ' 1 | ' 1 1 1 | 1 11 > | 279 > I | rl — ' i 11 ■ ■ i ■ • ■ ■ i 1 ■ ■ ■ i ■ ■ ■ ■ i ‘ ‘ ' i ■ ' ■ ■ i ■ 1 1 1 i ' ' 1 ' i ' 1 I ' ' ' ' l ' 1 ' ‘ I n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 31.00 31.20 31.40 31.60

12477.D 052202.M Mon Jun 03 11:39:36 2002 Page 21

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