GCMS quantitation report, sample AE11933, June 2002

NYC 9/11 Public Portal Document Library searen Compound Report

. Data File : C:\MSDCHEM\1\DATA\0610022\11933.D Vial: 10 Acq On : 10 Jun 2002 6:21 pm Operator: Sample : gc/ms scan 6/7 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NI ST9 8 . L . ********************************************************************* Peak Number 10 Decane, 2,5,6-trimethyl- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 8.70 0.21 ug/L 174815 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decane, 2,5,6-trimethyl- 184 C13H28 062108-23-0 59 2 2,2,7,7-Tetramethyloctane 170 C12H26 001071-31-4 50 3 Heptane, 2,2,3,4,6,6-hexamethyl- 184 C13H28 062108-32-145 4 Heptane, 2,2,4-trimethyl- 142 C10H22 014720-74-2 45 Abundance Scan 957 (8.702 min): 11933.D (-952) (-) m/ z 57.10 100.00% 57

5000

— 43 85 1 99 71 8.40 A

8.60 8.80 -4900 0 ... l... ^.,..1 ----- m/z 56.10 46.02% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #16364: Decane, 2,5,6-trimethyl- 57 43

5000 i • ■ ■ ■ i 1 ■ ■ ■ i 8.40 8.60 8.80 9.00 71 m/ z 43.10 30.26% 84 — 0- rprm mad — Ijimo 111111 ‘1’1’1’11 .88, 113 127 150 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #16840:2,2,7,7-Tetramethyloctane 57 MAMdhukuuliLMdaMYi 8.40 8.60 8.80 9.00 5000 m/z 41.10 24.65% 41 29 71 85 ml ....I......... .................... ..................... niz-> 0-

Abundancei 11"0111111111111110711/37711321177271"2212121‘8‘22111221110—0—23T53721"T :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200

57 #16859: Heptane, 2,2,3,4,6,6-hexamethyl- MmMnm 8.40 8.60 8.80 9.00 m/z 71.10 21.56%

5000 43 71 85

z—> 0 .4 29 | , 1 | 97 113 -rrpT ' i ‘ ■ ■ ■ I ■ ■“!111111''11"111 127 197 '111111111 “ “ I"111"111" " 111111"111"1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ....... 1........ 1, 8.40 8.60 8.80 9.00

11933.D 060302.M Tue Jun 11 08:23:14 2002 Page 13

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