GCMS quantitation report, sample AE11933, June 2002

NYC 9/11 Public Portal Document Library yearen compound Report

. Data File : C:\MSDCHEM\l\DATA\0610022\11933.D Vial: 10 Acq On : 10 Jun 2002 6:21 pm Operator: Sample : gc/ms scan 6/7 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 2,5-Dihydrophosphole, 3-met... Concentration Rank 10 R.T. EstCono Area Relative to ISTD R.T. 22.54 0.25 ug/L 305875 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-Dihydrophosphole, 3-methyl-l ... 192 C11H13OP 1000196-97-5 53 Q 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 53 /) 3 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 42 4 Pyrazine, tetraethyl- 192 C12H20N2 038325-19-8 42 Abundance Scan 3312 (22.539 min): 11933.D (-3300) (-) m/z 192.10 100.00% 192

5000

146 160 A 42 O+ —DTTTTTTTTT PHPTP “I' .'I. I 70 82 f 118 4' " ■!' "-I ■ - 22.20 22.40 22.60 22.80 m/z 191.00 24.81% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- 192 164

5000 99 115 ..... n...... 22.20 22.40 22.60 22.80 47 77 177 m/z 146.10 14.67%

mZz-> Abundance 0 44 + 67 1,57 1, +87+++ 4.34.,444155, Hmm 125,2 146 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #125847: Anthracene, 2-methyl- u 192 -A ' i • ■ •1* i 22.20 22.40 22.60 22.80 5000 m/z 193.00 13.17%

28 39 51 63 82 86 ns 126 139 152 165 176 O TITTmmptmpThHm Wrr miz-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130140 150 160 170 180190 200 #80870: Thiocyanic acid, 2-benzothiazolyl ester 192 ...... )..... A, 22.20 22.40 22.60 22.80 m/ z 96.00 12.51% 5000

45 69 90 1°8 134 148 160 122 /z-> 0 ' l “ “ I " " I' I1" 1" .. 1,... 111 i' “ h11" 11111111"11" " i 1..... 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 " ‘ 1 * 22.20 22.40 22.60 22.80

11933.D 060302.M Tue Jun 11 08:23:16 2002 Page 14

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