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GCMS quantitation report, sample AE11933, June 2002

Machine-extracted title · confidence 100%

Quantitative analysis report for polycyclic aromatic hydrocarbons using gas chromatography-mass spectrometry from June 2002.

NYC-WTC_000015725–000015737

Folder label: “GCMS X 6/7/02 A 6/10/02

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NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\MSDCHEM\l\DATA\0610022\11933.D Vial: 10 Acq On : 10 Jun 2002 6:21 pm Operator: Sample : gc/ms scan 6/7 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 12 Phenanthrene-diO Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 23.06 0.30 ug/L 360410 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-diO 188 C14D10 001517-22-2 86 2 Anthracene-dlO- 188 C14D10 001719-06-8 64 3 Pentacyclo [7.3.1.1. (4,12) .0(2,7) .. . 188 C14H20 1000215-61-8 45 4 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 36 Abundance Scan 3401 (23.062 min): 11933.D (-3395) (-) m/z 188.10 100.00% 188

5000 - 80 94

miz-> 40 52 66 I 132 160 , 0 ' 11" 11"1' I “ “ I" " 11 ‘111111 “11111 “ I ‘" 11' " i ■ ■ ■ ■ i ■'' ‘ i1'1 -I’TTT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 U 22.80 23.00 23.20 23.40 m/z 189.10 17.28%

Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 m/z 94.00 15.89% 80 94 160 30 42 52 66 , 0 I" " I" " I ■'1' 11" ■ i111' i 111 ■' l'1 11 ++198 118. .132.146 +.1791794 W- iz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 - 22.80 23.00 23.20 23.40 5000 m/z 80.10 15.88%

80 94 160 , . 17 30 42 52 66 , 108118 132 146 t|.| 170179 0 ■ i *■‘11‘ i ■ TI i 11 n!IH!11111 11 I! H 1111 11 TTTHag miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )tetradeca... 188 22.80 23.00 23.20 23.40 m/z 184.10 13.84%

5000 79 91

ins 131 100 117 0‘i ।11'111"111 “ 11' । — 145.158173.. Il z—> 10 20 30 40 50 60 70 80 90 1K) 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11933.D 060302.M Tue Jun 11 08:23:17 2002 Page 15

NYC-WTC_000015736

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NYC-WTC_000015736Source: NYC Law Department, mirrored locally

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