GCMS analysis results for sample AE11417, May 2002

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Laboratory report of GCMS analysis for sample AE11417 conducted on May 30, 2002, showing surrogate recovery data.

NYC-WTC_000025371–000025385

Folder label: “GCMS X 5/16/02 A 5/20/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052002\11417.D Vial: 7 Acq On : 20 May 2002 6:10 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.44 ug/L 512238 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 90 2 Anthracene-d10- 188 C14D10 001719-06-8 87 3 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) . . . 188 C14H20 1000215-61-8 45 4 Pentacyclo[8.4.0.0(3,7) .0 (4,14) .... 188 C14H20 1000099-27-2 33 Abundance Scan 3409 (23.109 min): 11417. D (-3401) (-) m/z 188.15 100.00% 188

5000

66 80 94 158 22.80 23.00 23.20 23.40

mfe-> 0 111 " 11 40 | 111111111" 111111 TTT -H 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 i ■ " 11 ■ । 11. ■ I i |।. m/z 189.10 19.72% Abundance #79827: Phenanthrene-d10 188

5000 / 1’I’11114111’I’II 22.80 23.00 23.20 23.40 80 94 m/ z 80.05 16.12% 160 30 42 52 66 108 118 132 146 | 170179|,| 0— 111111 [ I mri [ rtfrf 111111 । । [ t i । I । i n ! p i । i FErit TITTrthrdi 1111111 11’l iz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 V 1 I ' 1 ' 1 I ' ‘ ' I 22.80 23.00 23.20 23.40 5000 m/z 94.05 12.42%

80 94 160 17 30 42 52 66 . 11 108 118 132 146 |L| 170179|,i 0 TyrrTTp-rTTp-rTTy+TTryH-r । [ 111111111 — t ] 11 j । ] I j । 11 11 it 1111 111111111 11 111 H |'i । 11 । 11 111'l'Pl IIII m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )]tetradeca... 188 22.80 23.00 23.20 23.40 m/z 184.05 11.71%

5000 79 91 55 67 131

0 Tll - 145 159 1 73 1" '11 I ' ' ' ' I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11417.D 050102.M Thu May 23 10:45:25 2002 Page 9

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GCMS analysis results for sample AE11421, May 2002 · Box DEP Box 18

NYC-WTC_000025447

Laboratory report showing GCMS results for sample AE11421 analyzed on May 30, 2002.

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