GCMS analysis results for sample AE12092, June 2002

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Laboratory report documenting GCMS analysis of sample AE12092 conducted on June 5, 2002.

NYC-WTC_000013603–000013623

Folder label: “GCMS X 5/22/02 A 5/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\12092.D Vial: 13 Acq On : 23 May 2002 7:45 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library :. C:\DATABASE\NIST98.L ****************************************************************** * * * Peak Number 12 Phenanthrene-diO Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

23.07 0.27 ug/L 252671 Phenanthranene-dl0 22.91 •

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 86 2 Anthracene-dlO- 188 C14D10 001719-06-8 80 3 Pentacyclo(7.3.1.1. (4,12) .0 (2,7) ... 188 C14H20 1000215-61-8 45 4 4-Methyl-2-(3-fluorophenyl)pyrim... 188 C11H9FN2 076128-66-0 42 Abundance Scan 3402 (23.068 min): 12092.D (-3395) (-) m/z 188.10 100.00% 188

5000

niz-> 40 52 66 80 0'l | l . > I J 1 I I . J l > I I J ! 1 I I | I . . . J . . J . J . . . i | . I I I J 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 94 “ i“ ■■ i“ “ i ' i" " i ■ ■ m158 । । m/z 22.80 23.00 23.20 23.40 80.10 14.35% Abundance #79827: Phenanthrene-d10 188

5000 13I T 22.80 23.00 23.20 23.40 m/z 189.10 13.85% 80 94 160 , 30 tt42 52 h । rl661111111 n 11111 ntrt108118 | 1111111 132 146 11 170179/ i! 11 ii i-[ 111111 ii TTNTTTTTTTT O IWIIIN117T n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 188

22.80 23.00 23.20 23.40 5000 m/z 184.10 13.78%

66। 80 94 160 . 17 30 , 42 52 J 108118 132 146 rI 170179 0- —mpmnpmodtmon—knm । ri lip 111 [ 1111| 11111111111111111111'1111111 l'i । 11 I ’f infill I1"Hnferar mfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79715: Pentacyclo|7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... 188 22.80 23.00 23.20 23.40 m/z 94.00 13.07% 5000 79 91 55 67 ins 105 117 131 145 159 0-ppmpt 173‘ ’ 1' *' 1 trrrr »I wlmmt / 1 /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

12092.D 052202.M Wed May 29 09:52:20 2002 Page 15

NYC-WTC_000013622

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