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GCMS analysis results for sample AE10816, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS analysis results for sample AE10816 including surrogate recovery data on May 14, 2002.

NYC-WTC_000023502–000023516

Folder label: “GCMS X 5/9/02 A 5/13/02

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Scanned page image, NYC-WTC_000023515
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\10816.D Vial: 13 Acq On : 13 May 2002 9:16 pm Operator: Mclean Sample : 5/9 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 6 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.53 ug/L 686561 Phenanthranene-dl0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 90 2 Anthracene-diO- 188 C14D10 001719-06-8 87 3 4-Methyl-2-(3-fluorophenyl)pyrim... 188 C11H9FN2 076128-66-0 40 4 Antipyrine 188 C11H12N2O 000060-80-0 40 Abundance Scan 3409 (23.109 min): 10816.D (-3403) (-) m/z 188.10 100.00% 188

5000

80 94 156 | 22.80 23.00 23.20 23.40 42 54 66 253 Ot i I I | I I I I ["i : [ “■' ! 111 'l "l’It1 >11 > | | 136 I I | : —-l ■ ■ i m/z 189.10 17.89% /z-> 20 40 60 80) 100 120 140 160 180 200 220 240 Abundance #79827: Phenanthrene-d1 0 188

5000 ------------- 22.80 23.00 23.20 23.40 m/ Z 80.10 17.30% 80'94 160 , 01 ,1/28/40,5266.1. ,01l, 198129132 146. 1.... Jl,11 ‘ 1 [ > 1 ‘ I 1 ' ' • I m/z-> 20 40 60 801 100 120 140 160 180 200 220 240 Abundance #79826: Anthracene-d10- 188 ------- 22.80 23.00 23.20 23.40 5000 m/z 184.10 16.23%

80 94 160 OTTmuB—gutr 1lsi]. l, 106118 132 146. , ...4........ .... 28 40 52 66 miz—> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #79744:4-Methyl-2-(3-fluorophenyl)pyrimidine /1 188 22.80 23.00 23.20 23.40 m/ z 94.00 13.61%

5000 121

173 0 52 67 ,82 94I, 108 I. 134146 161 39 0U^ —TTt TT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 22.80 23.00 23.20 23.40

10816.D 050102.M Tue May 14 11:43:05 2002 Page 9

NYC-WTC_000023515

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NYC-WTC_000023515Source: NYC Law Department, mirrored locally

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