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GCMS analysis results for sample AE09568, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE09568 conducted on May 15, 2002.

NYC-WTC_000022916–000022929

Folder label: “GCMS X 5/8/02 A 5/10/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\050902\9568.D Vial : 23 Acq On : 10 May 2002 10:02 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHDDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.46 ug/L 714360 Phenanthranene- dl 0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 80 2 Anthracene-dlO- 188 C14D10 001719-06-8 59 3 Benzene, 1-(1-cyclohexen-l-yl)-4.. 188 C13H160 020758-60-5 58 4 Antipyrine 188 C11H12N2O 000060-80-0 50 Abundance Scan 3409 (23.109 min): 9568.D (-3402) (-) m/z 188.10 100.00% 1(18

5000

94 — 80 42 54 66 , 22.80 23.00 23.20 23.40 . 108 9 111111111111 THH +mmmmmm—TTT 132 146 158 11 m/ z 94.10 17.10%| mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 1(18

5000 m 22.80 23.00 23.20 23.40 80 m/z 189.20 14.32%| 94 160 30 42 52 66 0 mT II ITTTTITI I I I | II 11 | I I I I | ! I I'! +108.118 132.146—4179179— TTTT 11 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d1 0- 1(8

22.80 23.00 23.20 23.40 5000 m/z 184.10 14.20%|

80 94 160 , . 17 30 42 52 66 108118 132 0 TIPOTTTTTTTT 11111111111 11111 "l""i 146—4+179179— ‘I n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79791: Benzene, 1-(1-cyclohexen-1-yl)-4-methoxy- . ............................... 1(8 22.80 23.00 23.20 23.40 m/z 80.00 12.11%

5000 160

77 91 115 129 145 173 41 5165 102 0 11" " 11111 ]11" ‘ Hr ull "T''1" I m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

9568.D 050102.M Mon May 13 11:44:51 2002 Page 7

NYC-WTC_000022927

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NYC-WTC_000022927Source: NYC Law Department, mirrored locally

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