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GCMS blank analysis results, June 5 2002

Machine-extracted title · confidence 100%

Laboratory report showing non-detect levels of volatile organic compounds in a GCMS blank sample analyzed on June 5, 2002.

NYC-WTC_000015496–000015523

Folder label: “GCMS X 6/4/02 A 6/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060402\604LB.D Vial: 3 Acq On 4 Jun 2002 5:29 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 16 Phenanthrene-diO Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.24 ug/L 181334 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual ~ 1 Phenanthrene-diO 188 C14D10 001517-22-2 7214 2 Anthracene-d10- 188 C14D10 001719-06-8 72— 3 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 40 4 Antipyrine 188 C11H12N2O 000060-80-0 9 Abundance Scan 3401 (23.062 min): 604LB.D (-3395) (-) m/z 188.10 100.00% its

5000 .................. ........................ ............ 80 94 158 . 22.80 23.00 23.20 23.40 0 111111111140 ...... pjp.jU ------ ITT m/z 80.10 20.77% miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 US

5000 22.80 23.00 23.20 23.40 m/z 189.10 19.86% 80 94 160 42 n 52 30 11111 66 . 108118 132 11 -146 , |, 170179,1 0-HyrrTtp-rrTp-r T TTHIPTTTTTTTT 111 n } i! I j ।j > H 1111 [ mz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79826: Anthracene-d1 0- 188 ................... ........................... 22.80 23.00 23.20 23.40 5000 m/z 94.00 18.19%

RR 80 94 160 , , 17 30 42 52 66 , „ 108118 132 146 ,|,| 170179,1 0- 111 ‘ ‘ 1'''11" " 111 “T*111 [ I “ 1 H 1 TThmm niz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance> #79791: Benzene, 1 -(1 -cyclohexen-1 -yl)-4-methoxy- US 22.80 23.00 23.20 23.40 m/z 184.00 15.31% 5000 160

115 129 145 173 41 51 65 77 91 102 II I i -[MU । rJt 0 THulmal HHr ^4'11 "4TTur /1 miz—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

604LB.D 060302.M Wed Jun 05 12:28:53 2002 Page 19

NYC-WTC_000015518

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NYC-WTC_000015518Source: NYC Law Department, mirrored locally

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