GCMS analysis results, sample AE09331, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\050902\9331.D Vial: 21 Acq On : 10 May 2002 8:24 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 7 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.51 ug/L 891875 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 87 2 Anthracene-dlO- 188 C14D10 001719-06-8 64 3 Cycloheptanone, 4 -phenyl- 188 C13H160 067688-28-2 50 4 Antipyrine 188 C11H12N2O 000060-80-0 50 Abundance Scan 3409 (23.109 min): 9331 .D (-3402) (-) m/z 188.10 100.00% 188

5000

80 94 43 57 66 108 132 146 160 l 22.80 23.00 23.20 23.40 0 TH IRi 11 i~i~i |'i, । ij n'i । pl 1111 i 'f i I I i i । i I t । i I i । i 1 । i | । i । / /1 i । rp । । । । i । ] l’i I I | i । i 11 m/ z 94.10 18.46% m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 ryrPri r j i i i । । ■ । । i । 22.80 23.00 23.20 23.40 m/z 80.10 14.91% 80 160 30 42 52 68 108118 132 146 1 170179 0 TLUTTTTTTTTTTTTTTTTTHTTTTTHTT I | > I I IJ I I I t | I I ■ I | I I II | I I I ITrTTI!’ | ■ | | r i | ■ [ ITII 1 i I 1111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d 10- 188

22.80 23.00 23.20 23.40 5000 m/z 189.10 12.94%

160 80 , .94 66 17 30 42 52108 118 132 0 ''I'"....... ..... .................... .. ■ I ■> 1.1.. il i 1111 rt । f ri fTTttttr 146,111.179179,., mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- ■ ■ i 1 ' I 1 ' 1 ' 1 ‘ ' I 1tS 22.80 23.00 23.20 23.40 117 m/z 184.10 12.55% 104 91 160 5000 131 170 27 u 39 51 65 78 145

n/z-> — I4HHHH+ + 0 'l'"'I"111!1 — 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 ........ ..... . 22.80 23.00 23.20 23.40

9331.D 050102.M Mon May 13 11:42:39 2002 Page 10

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