GCMS blank analysis results, June 5 2002

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Library Search Compound. Report Data File C:\MSDCHEM\1\DATA\060402\604LB.D Vial: 3 Acq On 4 Jun 2002 5:29 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C: \MSDCHEM\1\METHODS\060302 .M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 17 Carbazole, 1,5,7-trimethyl- Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 34.85 0.26 ug/L 80366 Perylene-dl2 34.65 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Carbazole, 1,5,7-trimethyl- 209 C15H15N 1000138-13-9/5 2 4-Benzylidene-1-phenyl-3,5-dioxo... 264 C16H12N2O2 015083-26-8 5 3 1-Methanesulphonyl-5-fluorouracil 208 C5H5FN204SI 054391-00-3 5 4 2-Propenoic acid, 3-(3,4-diethox... 264 C15H20O4 075332-49-9 5 Abundance Scan 5407 (34.848 min): 604LB.D (-5406) (-) m/z 263.20 100.00% 263

130 209 5000 ) * 1 1 1 ' 1 'i ***I’’ 40 34.60 34.80 35.00 35.20 0- m/z 264.10 86.55% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #85318: Carbazole, 1,5,7-trimethyl- 209

5000 194 34.60 34.80 35.00 35.20 m/z 130.20 62.76% 40 51 63 84 102 115 127 139 152 165 178 0- ■ ■ i ■ ■1 ■ *1 "fi Ti ■ r'* • ■i r"t IITI । "r1 ‘'"I"1 r"" i 4" 1 ■ i 1 • 1 ■ i ■ • • ■ i ■ ■ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #95087:4-Benzylidene-1 -phenyl-3,5-dioxopyrazolidine 264

34.60 34.80 35.00 35.20 130 m/z 259.00 61.03% 5000 77 102 195 51 63 , 91 158 173

miz-> 01 jaabaalyun% 40 60 80 hi l|l 100 120 140 160 180 200 220 240 260 ,, I, , , ,i, , , I,

Abundance #58995:1-Methanesulphonyl-5-fluorouracil 130 34.60 34.80 35.00 35.20 m/z 208.90 53.45%

5000 79 208 A 31 42 58 100 114 143 0 4, ■ ml Jitv - n/z—> 40 60 80 100 120 140 160 180 200 220 240 260 34.60 34.80 35.00 35.20

604LB.D 060302.M Wed Jun 05 12:28:54 2002 Page 20

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