GCMS analysis results for sample AE11928, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11928.D Vial: 8 Acq On : 23 May 2002 3:40 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 15 5,9-Methanobenzocyclooctene... Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 34.87 0.25 ug/L 124909 Perylene-dl2 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 5,9-Methanobenzocyclooctene, 3-c... 260 C17H21C1 058241-05-7 9 2 Carbazole, 1,5,7-trimethyl- 209 C15H15N 1000138-13-9 5 3 N-Cyclohexyl-2-furancarbothioamide 209 C11H15NOS 1000147-69-3 5 4 Carbazole, 2,4,6-trimethyl-_________ 209 C15H15N 1000138-14-2 5 Abundance Scan 5410 (34.866 min): 11928.D (-5408) (-) . m/z 260.10 0.00% 260 128 209 84 191 5000 44 34.60 34.80 35.00 35.20 0- ■ ■ i ■ ■ ■ ■ । ■ ■ i ■ ■ • ■ i ■ ■ i • • • ■ i ■ ‘ ■ i ■ ■ ■ ■ i • • ■ i ■ • ■ • i ■ ■ H m/ Z 128.00 69.74% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #1526:5,9-Methanobenzocyclooctene, 3-chloro-5,6,9,10-tetr... 4h

29 5000 245 260 53 115 34.60 34.80 35.00 35.20 65 77 91 128 141153, 191 m/z 209.00 67.16% 15 165 178 0- — I ill,.d , III,, I rnfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #85318: Carbazole, 1,5,7-trimethyl- 209

34.60 34.80 35.00 35.20 5000 194 m/z 83.90 61.99%

51 63 84 102 115127139 152 165 178 0- ——Pmmtpttr ■ ■ i ■ 1 ■ 11‘ ■ 1 ■ i ' ■ miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #85256: N-Cyclohexyl-2-furancarbothioamide 11 1 128 209 34.60 34.80 35.00 35.20 m/z 1,91.00 59.04% 5000 39 94

55 67 176 1 .. 81 . 141 0 li, I i 111 1 1 1 11 111 ■ ■ i ■ ■ ‘ • i ' ■ i1 1 । •1 ■ ■ । ■ ■ ■ ■ ।1 ■ ■ ■ । ■ "I 1 ■ i ’ ■ n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 34.60 34.80 35.00 35.20

11928.D 052202.M Wed May 29 09:48:56 2002 Page 18

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