GCMS analysis results, sample AE12478, June 2002

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Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052902\12478.D Vial: 20 Acq On : 30 May 2002 1:34 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98. L Peak Number 16 Phenanthrene-diO Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.32 ug/L 353573 Phenanthranene-dl0 22.91 Hit# Of 5 Tentative ID MW MolForm CAS# Qual A 1 Phenanthrene-diO 188 C14D10 001517-22-2 87 y 2 Anthracene-dlO- 188 C14D10 001719-06-8 86 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 Abundance Scan 3401 (23.062 min): 12478.D (-3394) (-) m/z 188.10 100.00% 188

5000

80 94 22.80 23.00 23.20 23.40

m/z-> 43 57 66 0 TTUTIPTTTTTWTT „Aal..pamar.. .132.071s 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 ‘I m/z 94.05 16.15% Abundance #79827: Phenanthrene-d10 188

— 5000 22.80 23.00 23.20 23.40 m/z 80.10 15.93% 80 94 160 30 42 52 66 , 132 146 1I. 170179,1,1 o TICUICBuHh h M 1111 [ H 111! i108118 ,]| ! > 1111 i । m r|'l i Iaafiju n r| 11111IH1! ITT ■n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 108

22.80 23.00 23.20 23.40 5000 m/z 189.10 15.80%

RR 80 94 . 160 . i 17 30 42 52 66 niz-> 0-nmaapmgHHtt +108 118.132.146179179 — 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 22.80 23.00 23.20 23.40 m/ z 92.10 10.04% 145 5000

41 51 63 77 89 102 117 130 159

miz-> 01 ZjI. 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160170180 190 22.80 23.00 23.20 23.40

12478.D 052202.M Mon Jun 03 11:40:47 2002 Page 19

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