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GCMS analysis results, sample AE12476, June 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE12476 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014406–000014432

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document . Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052902\12476.D Vial: 18 Acq On : 29 May 2002 11:56 pm Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 17 Phenanthrene-diO Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.34 ug/L 386262 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID Qual MW MolForm CAS# 1 Phenanthrene-diO 188 C14D10 001517-22-2 940 2 Anthracene-diO- • 188 C14D10 001719-06-8 9327 3 2-Quinolinecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 40 4 Cycloheptanone, 4-phenyl-188 C13H160 067688-28-2 37 Abundance Scan 3401 (23.062 min): 12476.D (-3395) (-) m/z 188.10 100.00% 188

5000

80 94 43 57 66 । 132 146 158 22.80 23.00 23.20 23.40 0-TmTTTTHTHhH mpp Trrrr m/z 94.10 18.32% mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 -PPP- 22.80 23.00 23.20 23.40 80 m/z 189.20 15.61%| 94 160 30 42 52 66 1 108118 132 146 1 170179,1,1 | ' 0 TIPmmIOnHhtnt; M n {1! 11 {rn »111 it J1111{ r»111 1"‘f"TT miz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 1(8

22.80 23.00 23.20 23.40 5000 m/ z 80.10 15.15%!

„ 80 94 160 । 17 30 42 52 P . 1 108 118 132 146 II 1701791 0 'i |i m n 1111 < i it; l n : ]! l n । ill 11 ri 111! m r| H n ।»> 111 n ityrt 111! 11 iji t !i| n ni|mi NHMt mi miz-> 10 20. 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #125696:2-QuinoIinecarboxaIdehyde, 8-hydroxy-, oxime — 1(8 22.80 23.00 23.20 23.40 rn/z 184.10 14.35 5000 143 . 89 115 . 51 64 76 | 102 | 130 ,| 158 170 m/z—> 0- -HH TTm 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

12476.D 052202.M Mon Jun 03 11:34:21 2002 Page 20

NYC-WTC_000014430

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NYC-WTC_000014430Source: NYC Law Department, mirrored locally

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