GCMS analysis results, sample AE12476, June 2002

NYC 9/11 Public Portal Document . Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052902\12476.D Vial: 18 Acq On : 29 May 2002 11:56 pm Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 18 Naphthalene, 1,2,3,4-tetrah... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

34.79 0.62 ug/L 329735 Perylene-d12 34.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Naphthalene, 1,2,3,4-tetrahydro-.. . . 244 C18H28 029138-91-8 23 2 lH-Indene, 2,3-dihydro-1,3-dimet... 146 C11H14 004175-53-5 17 3 Benzaldehyde, (phenylmethylene)h... 208 C14H12N2 000588-68-1/9 4 4,5-Diphenylocta-1,7-diene(dl) 262 C20H22 1000215-92/8 9 Abundance Scan 5397 (34.790 min): 12476.D (-5396) (-) m/z 131.60 100.00% 131

5000 -.......... 73 86 51 116 208 257 34.40 34.60 34.80 35.00 35.20

niz-> 0- . Ia.,4 20 40 60 — ■ । ■ ■ ■ ■ । 80 100 120 140 160 180 200 220 1 ■ । ■ ■ ■11 ■ 240 260 m/z 130.90 30.75% Abundance #59322: Naphthalene, 1,2,3,4-tetrahydro-1-octyl- 131

5000 ........... A ' i ■ ■ ■ ■ i ■ AMA 34.40 34.60 34.80 35.00 35.20 91 m/z 132.60 28.65% 244 0 n/z->______ 20 15,22.11,53,65 40 60 77.,1,102115, 80 — 145157169 . |T 187 209 | . 7. | .... 1 . — 100 120 140 160 180 200 220 240 260 Abundance #59366:1H-lndene, 2,3-dihydro-1,3-dimethyl- 131

34.40 34.60 34.80 35.00 35.20 5000 m/z 73.10 27.60% 146 91 115

niz-> 0- ..2 39,51,54,77.1. 193,1...... '....................... k * ' I ‘ 1 1 ‘ 1* » ’ 1 • * » * ( J » * > I » I fI I » J I » I i I I J I I » 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #121981: Benzaldehyde, (phenylmethylene)hydrazone kikit 131 34.40 34.60 34.80 35.00 35.20 77 m/z 86.00 24.97% 5000 207 51 104 180 27 39 63 , 89 n/z-> 0 -4 — l80, h 100 . I, 117 I , | 1 152 165 J 192 1T"11 '' 1 ‘ ■ i ■ ■ ' ■ i ■ ■ ■ ■ i ■ • A wAANurwA Hssm, 20 40 60 120 140 160’ 180 200 220 240 260 34.40 34.60 34.80 35.00 35.20

12476.D 052202.M Mon Jun 03 11:34:23 2002 Page 21

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