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GCMS analysis results, sample AE09155, May 2002

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GCMS analytical report for environmental sample AE09155 including surrogate compound data from May 15, 2002.

NYC-WTC_000022857–000022878

Folder label: “GCMS X 5/8/02 A 5/10/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\050902\9155.D Vial: 20 Acq On : 10 May 2002 7:36 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 2-Propen-1-one, 3-(4-methyl... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

36.45 1.19 ug/L 612126 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propen-l-one, 3-(4-methylpheny... 222 C16H140 004224-87-7 17 2 Naphthalene, l-chloro-2,6-dimeth... 222 C12H11C1O2 025315-09-7 14 3 3-Buten-2-one, 4,4-diphenyl- 222 C16H140 000837-66-112 4 3-Buten-2-one, 4,4-diphenyl- 222 C16H140 000837-66-1 12 Abundance Scan 5680 (36.452 min): 9155.D (-5678) (-) m/z 207.00 100.00% 207

177 283

355 430 503 posw"Wuhtt 5000

149 36.20 36.40 36.60 36.80 74 I i m/z 222.10 87.25% /z—> 007 50 Abundance 100 150 200 250 300 350 400 #84905:2-Propen-1 -one, 3-(4-methylphenyl)-1-phenyl- 450 500

207

A 5000 145 105 36.20 36.40 36.60 36.80 179 m/z 221.10 86.40% 51 ob a il a | I + — miz-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #88163: Naphthalene, 1 -chloro-2,6-dimethoxy- 222 179 36.20 36.40 36.60 36.80 5000 m/z 283.00 71.10% 136

51 75 113 8+—44al4 28 0-- Ll— n/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #126958:3-Buten-2-one, 4,4-diphenyl- 221 36.20 36.40 36.60 36.80 178 m/z 193.00 60.62%

5000 43 105 77 152 0- . 44 4412844,4,4 — t— ‘ I ' ‘ 1 1 I ' ' "E ttt 'I i' n/z-> 0 50 100 150 200 250 300 350 400 450 500 36.20 36.40 36.60 36.80

9155.D 050102.M Mon May 13 11:41:48 2002 Page 15

NYC-WTC_000022876

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NYC-WTC_000022876Source: NYC Law Department, mirrored locally

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