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GCMS analysis results for sample AE11930, June 2002

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Laboratory report documenting GCMS analysis of sample AE11930 conducted on June 4, 2002.

NYC-WTC_000013551–000013573

Folder label: “GCMS X 5/22/02 A 5/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11930.D Vial: 10 Acq On : 23 May 2002 5:18 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 Naphthalene, 1,2,3,4-tetrah... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R-.T. 34.85 0.34 ug/L 115203 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Naphthalene, 1,2,3,4-tetrahydro- ... 208 C16H16 003018-20-0 9/ 2 1H-Indole, 6-methyl- 131 C9H9N 003420-02-8 5 3 Indolizine, 5-methyl- 131 C9H9N 001761-19-9/5 4 2-Propen-1-one, 1,3-diphenyl-, (E)- 208 C15H12O 000614-4771 5 Abundance Scan 5408 (34.854 min): 11930.D (-5406) (-) m/z 208.10 100.00% 11 8 208 259 131

5000 40 AAhputaalApnAqapuppyppbd 34.60 34.80 35.00 35.20

iz-> 0 40 +‘144*1*44+1*4*‘1‘ ‘*I*‘‘‘I‘+‘+I-‘‘‘IT 60 80 100 120 140 160 180 200 220 .. 240 1..., 260 m/z 117.90 92.86% Abundance #126509: Naphthalene, 1,2,3,4-tetrahydro-1-phenyl- 208 180

130 - 5000 34.60 34.80 35.00 35.20 165 m/z 259.00 82.77% 91i 104115 , 1,1,,.|ll 1.41 152 77 191 . 0 ------- Tt‘4714 ri t T » 14) h ■ I'1 ■ A1'. । Ml m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #122025: 1 H-Indole, 6-methyl- ................... ............................. 131

34.60 34.80 35.00 35.20 5000 m/z 131.50 68.91%

51 65 77 sg 103 0- ■ i । । il । 4, pap । p ■ dh . ( । . J niz-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #59295: Indolizine, 5-methyl- 131 34.60 34.80 35.00 35.20 m/z 265.20 66.39% 5000

51 65 77 103 ....... O' T-T I ll ,........1l | 1 I I I "J-! I I r | I I I I | I I I I | I > n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 34.60 34.80 35.00 35.20

11930.D 052202.M Wed May 29 09:50:24 2002 Page 17

NYC-WTC_000013572

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NYC-WTC_000013572Source: NYC Law Department, mirrored locally

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