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GCMS analysis results for sample AE09568, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE09568 conducted on May 15, 2002.

NYC-WTC_000022916–000022929

Folder label: “GCMS X 5/8/02 A 5/10/02

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Scanned page image, NYC-WTC_000022928
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9568.D Vial: 23 Acq On : 10 May 2002 10:02 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 3-Heptene(dithioic) acid, 6.. Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

34.91 0.62 ug/L 550663 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Heptene(dithioic) acid, 6-hydr... 232 C11H20OS2 083041-11-6 9 2 2-Methyl-6-phenylimidazo[2,1-b]-... 263 CllH9N3Se 1000211-79-9 9 3 4-Amino-4-cyano-3,5-dimethyl-2-p... 229 C14H19N3 1000216-11-1 9 4 1,4-Methanonaphthalen-9-ol, 1,2,... 202 C13H1402 001207-27-8 9 Abundance Scan 5417 (34.907 min): 9568.D (-5416) (-) m/z 263.10 100.00% 118 263 129

5000 104 232

.......................... 73 86 | — ............. 208 34.60 34.80 35.00 35.20 m/z 117.70 87.31% O+ TIT miz-> :20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #5876:3-Heptene(dithioic) acid, 6-hydroxy-6-methyl-, 1-me... 43 59

81 97 189 5000 232 34.60 34.80 35.00 35.20 131 m/z 129.10 77.61% 171

miz-> o! :20 4 27 1

40 Lh i i L Lu 4l I - ijt119 60 80 I r Ji 11 143 100 158

120 140 -Hl — ' ,44 '' 160 180 200 220 240 260 214 it

Abundance #95018:2-Methyl-6-phenylimidazo[2,1 -b]-1,3,4-selenadiazole 263 ' 1 1 * 1 1 34.60 34.80 35.00 35.20 5000 103 195 m/ z 260.10 49.50% 116 51 63 76 89 01 . I 1 !1. A t l t ..-H4HIr r1,1111 '111 - 168 . 130142 222 ' 101ml ' ' m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #52826:4-Amino-4-cyano-3,5-dimethyl-2-phenylpiperidine 1 8 34.60 34.80 35.00 35.20 91 m/z 130.90 44.78% 104 146 5000

n 203 41 . 187 56 132 0 TTir — I । Il । ll । I 41 h -I r [ I -++ 158 172 I ih । rlhi 1" । "" । | | 229 1 ■ i ■ ■ AA m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 34.60 34.80 35.00 35.20

9568.D 050102.M Mon May 13 11:44:51 2002 Page 8

NYC-WTC_000022928

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NYC-WTC_000022928Source: NYC Law Department, mirrored locally

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