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GCMS analysis results for sample AE11421, May 2002

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Laboratory report showing GCMS results for sample AE11421 analyzed on May 30, 2002.

NYC-WTC_000025447–000025463

Folder label: “GCMS X 5/16/02 A 5/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report I Data File : C:\MSDCHEM\1\DATA\052002\11421.D Vial: 11 Acq On : 20 May 2002 9:26 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 8 Phenanthrene-diO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.43 ug/L 490000 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID • MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 8 2 Anthracene-diO- 188 C14D10 001719-06-8 50= 3 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 42 4 4-Methyl-2-(3-fluorophenyl )pyrim... 188 C11H9FN2 076128-66-0 42 Abundance Scan 3409 (23.109 min): 11421.D (-3402) (-) m/z 188.10 100.00% its

5000 ........ / 94 ’ I’’’. r 1 1 1 1 ' 1 1 1 1 ■ ' I 43 57 66 80 132 160 22.80 23.00 23.20 23.40 0 -mmmmmmmmmm m/z 189.05 14.82%I mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 —uni mPr) | I I ! ! | 22.80 23.00 23.20 23.40 m/ z 94.15 13.94%| 80 94 160 42 u I52 66 30 m H 1 I I | I I 1 | | | 1-1 | | I I | | I I | I 108 118 132 146 , |.I 170179,1 0 11" " I'1" i ‘ TTTTTTTTTTTTTTTTTTTTITTTTTTTT mfz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d1 0- 188 ----- 22.80 23.00 23.20 23.40 5000 m/z 184.10 11.90%

80 94 160 , .

m/z-> 17 30 42 52 —889 0 1 r "' i1" ' i " " i1" ■ i1' ■ 66

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79745:4-Methyl-2-(4-fluorophenyl)pyrimidine - 1 ' 1 1 ' ' * 1 188 22.80 23.00 23.20 23.40 m/z 187.05 9.58% 121 5000 173 — 67 94 0 ' I " " I " " I " n39I • । | "57 1 84 |, 133 146 i-i p rl । i i'i 11 i 11 111 I'l r| I i n 11, 11 i1 161 , 1__ j " “I " '''1111 'I'1 rl ' 11 [ 11 p-rn I'1" m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11421.D 050102.M Thu May 23 10:48:27 2002 Page 11

NYC-WTC_000025462

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NYC-WTC_000025462Source: NYC Law Department, mirrored locally

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