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GCMS analysis results for sample AE11421, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS results for sample AE11421 analyzed on May 30, 2002.

NYC-WTC_000025447–000025463

Folder label: “GCMS X 5/16/02 A 5/20/02

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Scanned page image, NYC-WTC_000025461
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052002\11421.D Vial : 11 Acq On : 20 May 2002 9:26 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Anthracene, 2-methyl- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

22.58 0.29 ug/L 324810 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual N 1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 — 2 Bitoscanate 192 C8H4N2S2 004044-65-9 50 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 40 Abundance Scan 3319 (22.580 min): 11421 .D (-3308) (-) m/z 192.10 100.00%! 192

5000

- 82 96| 146 160

mz-> 43 70 . 0 ' i11111" 1' i'1 ‘" i " 111"111'1" i11'111" 11'1111" " 1111111 120 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 22.20 22.40 22.60 22.80 23.00 m/z 191.10 23.69% Abundance #125847: Anthracene, 2-methyl- 192

5000 TT TIr 22.20 22.40 22.60 22.80 23.00 m/z 146.10 15.92% 28 39 51 63 82 96 115 126 139 152 165 176 I 0 TPTTTTTTTTTggTTTTTTTTTTTTTt mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125828: Bitoscanate 192 ,........4........ 22.20 22.40 22.60 22.80 23.00 5000 m/z 193.10 15.54% 134 160 50 63 75 90 102 122 148 176 0 L111,111111111'i r‘ । rl’l’h r’lll— |-i'i rr’rrh 111 ih'i u 11 fl 11 ■ p1 T ponni r1111111' i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyl)- TI111411I ■ ■ i ■ ■ • ■ । ■ 192 22.20 22.40 22.60 22.80 23.00 161 m/z 96.20 12.2 6%I 5000

77 121 149 177 91 103 52 64 138

rdz—> 0 ' I " " I " " I " " P1, । > | r'l 1111' .. |.... Iasyilalyonan, 11'1" I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 L 22.20 22.40 22.60 22.80 23.00

11421.D 050102.M Thu May 23 10:48:26 2002 Page 10

NYC-WTC_000025461

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NYC-WTC_000025461Source: NYC Law Department, mirrored locally

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