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GCMS blank analysis results, sample AE09771, May 2002

Machine-extracted title · confidence 100%

Laboratory blank report for sample AE09771 showing non-detectable levels of target compounds from May 8, 2002.

NYC-WTC_000043869–000043880

Folder label: “GCMS X 4/25/02 A 5/7/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\l\DATA\050602\0425LB.D Vial: 16 Acq On 6 May 2002 11:56 pm Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 2 Anthracene, 2-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.58 0.31 ug/L 348630 Phenanthranene-dl0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 50 3 2,5-Dihydrophosphole, 3-methyl-l ... 192 C11H13OP 1000196-97-5 45 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 Abundance Scan 3319 (22.580 min): 0425LB.D (-3311) (-) m/z 192.10 100.00* 192

5000

TT Td TIT 146 160 82 96 22.20 22.40 22.60 22.80 23.00

lz—> 42 T 118 70 TH T -4i "'I..... ms...... ... 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 191.00 21.19% Abundance #125847: Anthracene, 2-methyl- 192

5000 22.20 22.40 22.60 22.80 23.00 m/z 193.00 14.79% 28 39 51 63 82 96 115 126 139 152 165 176 TITTTTTTTTTTTTTTTTTTTTTT i'I'i ri j > in । > 111 Mpt 1111111'| 1111 pi 111 t-ti । fl'i [ । r’l TTT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80950: 1,5-Naphthalenedithiole 192

22.20 22.40 22.60 22.80 23.00 5000 m/z 146.10 14.73% 115 128 159 40 57 147 69 79 96 1 06 I ------HH 11 p 11 , | I I,...... 1,1 h....... 177 I I | r i I I [ 111 III < " I" " I " 111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1 -oxo-1 -phenyl- ,..... ,4. 192 22.20 22.40 22.60 22.80 23.00 164 m/ Z 96.00 13.23%| A

5000 99 115 47 77 177 67 125 I46

m/z-> —2739 1.57. , +87++++ —HHIPP, I 11’111 i । ,134 | EE TIF —। ■1 1 । 1 1 1 1 ( 1 1 1 ' । ' 1। 1 । 1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

0425LB.D 050102.M Tue May 07 15:39:45 2002 Page 5

NYC-WTC_000043877

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NYC-WTC_000043877Source: NYC Law Department, mirrored locally

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