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GCMS analysis results for sample AE11384, May 22 2002

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Laboratory report showing GCMS analysis results for sample AE11384 conducted on May 22, 2002.

NYC-WTC_000025163–000025181

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\051702\11383.D Vial: 10 Acq On : 17 May 2002 8:07 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Anthracene, 2-methyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.58 0.33 ug/L 454448 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 45/ 2 2-Propenal, 3-(3,4-dimethoxyphen.. . 192 C11H1203 004497-40-9 42 ( 3 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 40. 4 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 40/ Abundance Scan 3319 (22.580 min): 11383.D (-3310) (-) m/z 192.10 100.00% 192

5000

42 54 120 70 82 96 146 160 । । ■ ■ ■ ■ t ■ 22.20 22.40 22.60 22.80 23.00 A "I ‘ ' ' ' I ‘

0 TTTTHTTTT ----- PTTT I " " I im+ti | I In | i i I ! | I M I1* I I I । i m/z 191.10 23 .97% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125847: Anthracene, 2-methyl- 192

5000 1 1 i 1 1 1 1 r1 1 TIT 22.20 22.40 22.60 22.80 23.00 m/z 146.00 15.10% 28 39 51 63 82 । 115 126 139 152 65 176 | 0-TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTCmWTTTHTHTTT n/z-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance। #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 ------- 161 22.20 22.40 22.60 22.80 23.00 5000 m/z 193.00 14.43%| 77 121 149 177 52 91 103 64 138 1111'111 i11" A nfe-> 0 ml.. I... I,. 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 r'11''11''' 'I'1'' 11111 [1'1

Abundance #125856: Phenanthrene, 1 -methyl- ‘ ' i ' ■ ' ' i ' 1 1 1 1 1 1 i 1 1 192 22.20 22.40 22.60 22.80 23.00 m/z 96.00 12.46%|

5000

96

■n/z-> 27 39 51 63 82 Il 115 126 139 152 165 178 , 0 1————- I*' 11 > i11" i "'" i" " r1M111 " I’11" i1,111111 Ih 11111 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 .]......... 22.20 22.40 22.60 22.80 23.00

11383.D 050102.M Tue May 21 11:55:27 2002 Page 9

NYC-WTC_000025176

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NYC-WTC_000025176Source: NYC Law Department, mirrored locally

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