GCMS analysis results for sample AE12092, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\12092.D Vial: 13 Acq On : 23 May 2002 7:45 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L *************************************** * ***************************** Peak Number 11 2-Propenal, 3-(3,4-dimethox... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.26 ug/L 245891 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9,42 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 38 3 Bitoscanate 192 C8H4N2S2 004044-65-9 38 4 Isoquinoline, 1,2,3,4-tetrahydro... 328 C18H20N2O4 1000128-79-2 33 Abundance Scan 3312 (22.539 min): 12092.D (-3304) (-) m/z 192.10 100.00% 192

5000

146 160 40 49 70 82 118 %6 22.20 22.40 22.60 22.80 0 i ‘ ■ * •11 ■ “ ‘ । m/z 191.00 19.91 mlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161

5000 22.20 22.40 22.60 22.80 77 91 121 149177 m/z 193.00 16.13% 52 64 103 138

miz-> 0 m—p I..I ■11 ■" ■ i ■ HHH 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 - H Abundance #80950:1,5-Naphthalenedithiole 192

22.20 22.40 22.60 22.80 5000- m/z 146.10 15.24 115 128 159 40 57 69 79 96 147

mfe-> 0- -------- ■ f‘i ■ ■■ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 +136, 177 " i ■ ■

Abundance #125828: Bitoscanate ojassir 11A r, J \ ‘ I ‘ 1 ‘ ‘ I 1912 22.20 22:40 22.60 22.80 m/z 96.00 12.10 5000 134 160

niz—> 0- .40150.1163.75,. 176 THTT ’ d 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 148 T’rTI’ 4 ‘ ‘ I ’ 1 1 • i ‘ I ‘ 1 ‘ ‘ I ‘ 22.20 22.40 22.60 22.80 4 * I

12092.D 052202.M Wed May 29 09:52:19 2002 Page 14

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