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GCMS analysis report sample AE09682, May 23, 2002

Machine-extracted title · confidence 95%

GCMS laboratory report for sample AE09682 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013258–000013276

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document Llprary search Compound Report

Data File : C:\MSDCHEM\1\DATA\052102\9682.D Vial: 18 Acq On : 22 May 2002 3:11 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 2-Propenal, 3-(3,4-dimethox. . . Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

22.54 0.28 ug/L 296480 Phenanthranene- dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 2 2 Bitoscanate 192 C8H4N2S2 004044-65-9/40 3 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15/8 36 4 Anthracene, 9-methyl-_______________ 192 C15H12 000779-02-2 36 Abundance Scan 3312 (22.539 min): 9682. D (-3302) (-) m/z 192.10 100". 00% 1912 I! /

5000

_ R2 96 146 160 22.20 22.40 22.60 22.80

m/z—> 42 54 0- THTTT 70 8- 118 1 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I m/z 191.10 18.97% Abundance #80953:2-Propenal, 3-(3,4-dimethoxypheny!)- 19/2 161

5000 22.20 22.40 22.60 22.80 77 121 149 177 m/z 146.00 15.02% 91 103

0 m .. |... I.. I, LH 52 64 138

niz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Ppur Abundance #125828: Bitoscanate 19/2 . .......................................... . 22.20 22.40 22.60 22.80 5000 m/z 193.10 14.38% 134 160 .,.^4..J.4r. 2,192.1.1122, 4 rd+p 0 148 /z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 176 '','1 ■ i"1 ■ i ■ “ ■ i

Abundance #81030:4-Hydroxy-3,5-dimethylcinnamicacid 192 22.20 22.40 22.60 22.80 m/z 160.10 11.51% 5000

89 175 45 55 I — 145

n/z—> 01 44++H+ +497,195, 117. 135 h, 163 T[+ i' d’r" 11 ■ 1' ■ IW’ i" " I1 - 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

9682.D 052202.M Wed May 22 11:46:56 2002 Page 11

NYC-WTC_000013273

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NYC-WTC_000013273Source: NYC Law Department, mirrored locally

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