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GCMS analysis results, sample AE09971, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09971 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000044071–000044093

Folder label: “GCMS X 4/25/02 A 5/7/02

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NYC 9/11 Public Portal Document

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Data File C:\MSDCHEM\1\DATA\050602\9977.D Vial: 19 Acq On 7 May 2002 2:22 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 9 2-Propenal, 3-(3,4-dimethox.. . Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 22.58 0.43 ug/L 408090 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenal, 3-(3,4-dimethoxyphen.. . 192 C11H1203 004497-40-9 42/ 2 2-Imidazolidinone, 1-methoxy-3-p.. . 192 C10H12N2O2 052420-43-6 >38 3 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 38 4 Anthracene, 9-methyl- 192 C15H12 000779-0X2 36 Abundance Scan 3319 (22.580 min): 9977.D (-3309) (-) ""m/z 192.10 100.00% 192

5000 ................. /............. ' i 1 1 1 1 1 1 ' ■ 1 1........... 1 1 1 40 96 146 160 70 82 22.20 22.40 22.60 22.80 23.00 120 -- I'1' ’ I ........ ‘"'I — 11 u " r ■ " 111 m/z 191.10 19.00% m/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- A 192 161

5000 22.20 22.40 22.60 22.80 23.00 m/ Z 96.10 —52 64 77• 91I . 121I 149 177 14.08%

/z—> ---------- 138 I 193 " 111 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 k.. I Abundance #80907: 2-lmidazolidinone, 1-methoxy-3-phenyl- 106 192

77 162 22.20 22.40 22.60 22.80 23.00 119 m/ z 40.10 13.89% 5000 42 56 91

m/z-> 28 4 +5 134 ]____ IIIT 111'111 r 1111 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1.. " " r 1 " I " " I " 111

Abundance #80950: 1,5-Naphthalenedithiole । । । । । । । । । । । । । । । । ।■ i । । । । । 192 22.20 22.40 22.60 22.80 23.00 m/z 146.10 12.178

5000 115 128 159 40 57 69 79 — 96 . 147 I 11 TOOI]uunuT I I 87 1 106 .1 V —TTtTTTT 11.... hL-i.., Bh.. 177 "r1 1.... . m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

9977.D 050102.M Tue May 07 15:54:24 2002 Page 13

NYC-WTC_000044088

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

NYC-WTC_000043938

Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

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