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← Document results/DEP Box 25/GCMS X 4/25/02 A 5/7/02
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GCMS analysis results, sample AE09971, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09971 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000044071–000044093

Folder label: “GCMS X 4/25/02 A 5/7/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050602\9977.D Vial : 19 Acq On 7 May 2002 2:22 am Operator: Mclean Sample 4/25 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 10 2-Quinolinecarboxaldehyde, . Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.58 ug/L 553972 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 2 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71- 40 3 Phenanthrene-dlO 188 C14D10 001517-22 37 4 Pentacyclo[8.4.0.0(3,7) .0(4,14) . . . . 188 C14H20 1000099- 7-2 33 Abundance Scan 3409 (23.109 min): 9977. D (-3402) (-) m/z 188.10 100.00% 188

5000

i-1 । । ii II 1 । 1 i'll i ] ! r 40 94 158 _ AA 80 22.80 23.00 23.20 23.40 11 " '' i " —57 H— I ! | ' I ! I | I > I > | > > I < | l ! < < | ' ' ! । | < I I I | I ' ! ! | I I ! ! | I I ‘r ... m/z 40.10 16.15% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188

5000 1 1 । 1 । । 1 I 1 । । । । । । । i । Cty 22.80 23.00 23.20 23.40 143 m/z 94.05 13.02% . 89 115 51 64 76 I 102 ! 130 .I1' 158 170 । । । । ' । [ । । । । । > i । । I'i । । i । i'rl । 1 >‘ll> । । i /I | i । ■ । । I i i i । । I'l'i । । । । I'l i i i • |'l i*rr|'r ... 11.. 1 H m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 - T ' | ' 1 ■ I | I I ' ' J

145 22.80 23.00 23.20 23.40 5000 m/z 158.10 11.60%

117 159 1 73 , 41 51 63 77 89 102 130 ------------- lb । i rlll'|'i i i i । I । . ......... . /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 3 1 [ I — Ton I ] I I I I I I I I I r

188 22.80 23.00 23.20 23.40 m/z 189.20 11.35%

5000

80 94 160

m/z-> 30 42 52 66 i | । i । । | i । । । | t r > । । I I I i । i I I i । i । !’ I

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 11 102110118 132 I i I I ( I I I I I I I I I I I I I I I I I I I I I I I I 146—4170.1804— TT 22.80 23.00 23.20 23.40

9977.D 050102.M Tue May 07 15:54:24 2002 Page 14

NYC-WTC_000044089

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NYC-WTC_000044089Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

NYC-WTC_000043938

Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

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