GCMS sample analysis results, AE11907, June 4, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.

NYC-WTC_000012989–000013013

Folder label: “GCMS X 5-21-02 A 5-22-02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11907.D Vial: 14 Acq On : 23 May 2002 12:25 am Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L ********************************************************************* Peak Number 13 Anthracene-dlO- Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

23.07 0.23 ug/L 200626 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 38 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 38 4 Phenanthrene-diO 188 C14D10 001517-22-2 38 Abundance Scan 3402 (23.068 min): 11907.D (-3395) (-) m/z 188.10 100.00% 188

5000

80 94 160 22.80 23.00 23.20 23.40 0 1.... 11144.11117.800112211/1/, 114***1****1***14***1** m/z 94.20 19.45% n/z-> 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 80.10 16.48% 80 94 160 17 30 42 52 66 t 108118 132 146 II. 170179 0 pr i | ri i > rrrt I'I. | If i! rrrtt t rrrt 111, | , i., 1111, i ii. |I. 11111111. ■ NIT77 rn T’TTn n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #125696:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188

22.80 23.00 23.20 23.40 5000 m/z 189.10 11.24%

51 6476 89 102 115 130 di 158 170 /z-> 0 ----- 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 TT Hm .............. ..................................... Abundance #79760:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 22.80 23.00 23.20 23.40 m/z 184.00 10.29%

5000

. 143 115 __ 39 50 63 158 170 77 89 103 || 130 ।

n/z—> 0 +H Tun 1111 > 111.. 11 > ।. i'i , * • * I1* * (** rl’i ■ i'i i'1'i 111 i'I'I 111 1 | I'I’I i , . I'I’. | I ■ ! Ifl-. I I |' 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 22.80 23.00 23.20 23.40

11907.D 052202.M Tue May 28 12:14:32 2002 Page 16

NYC-WTC_000013009

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NYC-WTC_000013009Source: NYC Law Department, mirrored locally

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