GCMS analysis results for sample AE10307, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10307.D Vial: 10 Acq On 8 May 2002 9:07 pm Operator: Mclean Sample 5/1 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 2-Propenal, 3-(3,4-dimethox... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.32 ug/L 446960 Phenanthranene-dlO 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenal, 3-(3,4-dimethoxyphen.. . 192 C11H1203 004497-40-9 42 0 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 40 y 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 40 / 4 Anthracene, 2-methyl- 192 C15H12 000613-12-7 40/ Abundance Scan 3319 (22.580 min): 10307. D (-3311) (-) m/z 192.10 100.00% 192

5000 ........ ........ / 3It1I|lr i i j i । I I | I t i I-

42 54 70 92 “ 96| 146 160 22.20 22.40 22.60 22.80 23.00 120 ' | ' 4# t , . | ! ||,I>| m/z 191.10 0 111111111 rrr’ttrrpi 11111111111111)! 1111'h —H 20.37% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161 - 5000 22.20 22.40 22.60 22.80 23.00 77 121 149 177 m/z 193.10 16.05% 91 103 52 64 138

m/z-> 0 ........... i... . ... I | I I I I | I I I I | I I I I | 1 I I I | I I ! 1 | I I >

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 .. ..I. I'1111 Up

Abundance #125842: Phenanthrene, 2-methyl- 192

22.20 22.40 22.60 22.80 23.00 5000 m/z 160.10 12.46%

96 27 39 51 63 82 1 115 126 139 152 165 176 0 ■ 11 < 11 11 111 । 11 ■ 111 i i ■ p' 11 11 i r 11 pi il| il'11 i | rri । 11 । । । । i i r।'। > ri i | I i । । । i'i i । । i ill । । h-rTp-r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125849: Anthracene, 9-methyl- .... ........... ...... 192 22.20 22.40 22.60 22.80 23.00 m/z 146.10 12.37%

5000

96 165 28 39 51 63 74 83 I 105 115 126 139 152 i 176 n 0- i । । । i‘l p j i <1j‘i । । । |‘i rri । l'ri ’ 1'17 Nh’l’rrl i'[ i iii I’l’ 1 । । i । । i i ri'i । । । । |'I । । । ; i1!1! । [ । rl'l [ । । i1!1 TI 1 i 1 1 ' ' I ' ' ‘ ' I ' ' mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

10307.D 050102.M Thu May 09 13:52:08 2002 Page 8

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