GCMS analysis results for sample AE10307, May 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10307 conducted on May 17, 2002.

NYC-WTC_000045155–000045170

Folder label: “GCMS X 5/1/02 A 5/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10307.D Vial: 10 Acq On 8 May 2002 9:07 pm Operator: Mclean Sample 5/1 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.58 ug/L 812212 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 78 • 2 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 50 p/ 3 Phenanthrene-diO 188 C14D10 001517-22-2 404 4 5 (4H)-Isoxazolone, 4,4 '-bi s [ 3 -me. . . 376 C22H20N204 128156-47-8/38 Abundance Scan 3409 (23.109 min): 10307.D (-3402) (-) m/z 188.10 100 /00% 188

5000

80 94 1 1 ' 1 1 1 1 1 1 1 I 42 54 66 iill 132 146 160 M 22.80 23.00 23.20 23.40 i ! i i | I' “TT 0- TTTTHTt Hir | I ■ i I | I > | I | I | i I | / I I I ITT# C| 1 I I "I’i I I I | I I I 1 J 1*1 II j m/z 94.05 17.86% m/z-> W 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 ........ / 1 ' i 1 1 ' 11 ‘ 1 i 1 1 ■ 1 i 1 1 1 1 i 22.80 23.00 23.20 23.40 m/z 189.10 15.53% 17 30 42 52 66 80 1 94 108118 132 146 160 1. 170179|,i A 0 1111111111 — i l’l"' i' i | i > > i | i i i i | I r । i | I 1 1—2041000111011110211101314181111 ’’’ 111 I M 111 rlT 100017 mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-pheny- 188 117 104 1 'T i ■ 1 1 1 i 91 22.80 23.00 23.20 23.40 160 5000 131 m/z 80.10 14.47%| 170 27 39 51 65 78 145

miz-> 0 * 11'111'' I’ n l'l n Hl. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TT Him 1 4 Abundance #79827: Phenanthrene-d10 188 22.80 23.00 23.20 23.40 m/z 184.10 10.67%| 5000

80 94 160 30 42 52 66 1 108 118 132 146 II 170179.1,11 |m/; 0 ————————— 1] THTT TTTTTTTTu Ti 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10307.D 050102 .M Thu May 09 13:52:08 2002 Page 9

NYC-WTC_000045168

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