GCMS scan data for sample AE11420, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052002\11420.D Vial: 10 Acq On : 20 May 2002 8:37 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 6 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD. R.T. 23.10 0.43 ug/L 583340 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 81 2 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 50 3 Phenanthrene-diO 188 C14D10 001517-22-2 50 — 4 1,3,5-Triazin-2-amine, 4,6-bis(m... 188 C5H8N4S2 030358-19-1 38 Abundance Scan 3408 (23.103 min): 11420.D (-3402) (-) m/z 188.10 100.00% 188

5000 ,..................... ............ 80 94 22.80 23.00 23.20 23.40 43 52 66 ----- J 132 146 160 —mmmmmhpmm m/z 189.20 15.58% 0— ।11111 TTTri mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1t8

5000 1 — । -PPr । । । । । 22.80 23.00 23.20 23.40 m/ z 94.10 14.80% 80 94 160 , । 66

mfe-> 17 30 42 52 0 . ............................... -# 146.4.1791794,—. 108 118 132 TTtut 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- 188

104 117 ..... U ‘ I’IIT’E ■ ■ i ' ' ' ' i

91 22.80 23.00 23.20 23.40 160 5000 131 m/ z 80.10 13.53% 170 27 39 51 65 78 145

mfa-> 0 . I, -+44+ 111" 111 ‘I 1 ++ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 - ....................................... . Abundance #79827: Phenanthrene-d10 US 22.80 23.00 23.20 23.40 m/z 184.10 10.46%

5000

80 94 160 30 42 52 66 11 108 118 132 146 ,|,I 170179 0 1»" 11 > ■" I'1" [1" ■ ।11 ■ ■ I ■11 ■ I" l-l |" ■' | I I i । [ I 11 r 11 ri 11 i 11 i |111 i । i i 11 11 tPl’r i 11 । 11 । । tH""t 11 । Ti ,.................................. m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11420.D 050102.M Thu May 23 14:07:11 2002 Page 9

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